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Nucleation and growth of twins in Zr: A statistical study

机译:Zr双胞胎的成核和生长:一项统计研究

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摘要

An in-depth statistical analysis using electron backscatter diffraction (EBSD) is carried out to expose statistical correlations between {101-bar 2} twinning and grain size, crystallographic orientation, grain boundary length, and neighbor misorientation in high-purity poly-crystalline zirconium strained to 5 and 10 at 77 K. A strong correlation was found between the active twin variant and crystallographic orientation. The propensity of a grain to twin or not was found to be only weakly dependent on grain area and diameter. Within the population of grains containing twins the number of twins per grain noticeably increases with grain area, and twin thickness is found to be rather insensitive to grain size and orientation. A weak preference for twinning was found for smaller grain boundary misorientation angles. These and the other statistical results reported can improve theoretical treatments for twin nucleation in polycrys-tal models. The statistical methodology presented has general applicability for all twin types in a wide range of metals.
机译:利用电子背散射衍射(EBSD)进行了深入的统计分析,揭示了在77 K下应变至5%和10%的高纯度多晶锆中{101-bar 2}孪晶与晶粒尺寸、晶体取向、晶界长度和相邻取向误取之间的统计相关性。发现活性孪生变体与晶体取向之间有很强的相关性。发现晶粒孪生与否的倾向仅与晶粒面积和直径微弱依赖。在含有孪生的晶粒群体中,每个晶粒的孪晶数量随着晶粒面积的增加而显著增加,并且发现孪晶厚度对晶粒大小和取向相当不敏感。对于较小的晶界取向错角,发现对孪晶的偏好较弱。这些和其他报告的统计结果可以改善polycrys-tal模型中双胞胎成核的理论处理。所提出的统计方法普遍适用于各种金属中的所有孪生类型。

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