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Effects of the heating history of impregnated lignocellulosic material on pore development during phosphoric acid activation

机译:浸渍木质纤维素材料加热历史对磷酸活化过程中孔发育的影响

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摘要

Activated carbon samples have been prepared by heating China fir (Cunnmghamia lanceolata) wood impregnated with phosphoric acid in an effort to elucidate the effect of the heating history of impregnated material on the porous texture of the activated carbon. Analysis of the pore structure of the activated carbon in terms of nitrogen adsorption isotherms showed that both using an intermediate isothermal treatment and slowing the heating rate up to 300 °C favor pore development but have a detrimental effect above 300 °C. Therefore, it is recommended that a two-step heating program is applied for phosphoric acid activation.
机译:通过加热浸渍磷酸的杉木(Cunnmghamia lanceolata)来制备活性炭样品,以阐明浸渍材料的加热历史对活性炭多孔纹理的影响。根据氮吸附等温线对活性炭孔隙结构的分析表明,使用中间等温处理和将加热速率减慢至300 °C有利于孔隙形成,但在300 °C以上会产生不利影响。 因此,建议采用两步加热程序进行磷酸活化。

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