Scanning Electron Microscope study of the exoskeletal ultrastructure of secondarily phosphatized material ofFlexicalymenesp. from the Upper Ordovician Maquoketa Shale, Iowa, USA, shows that the exocuticle, comprising 20 of the total exoskeletal thickness, is composed of horizontal laminar units between 0.2 and 1 μm thick. These units consist of primarily mineralized organic fibres which form horizontal laminae interconnected by inter‐laminae. The endocuticle is considerably more mineralized than the exocuticle, and its original organic structure cannot be observed in untreated preparations. Etching with chromium sulphate reveals: (1) horizontal organic laminar units, 0.2 to 2 μm thick, and (2) pore canals with non‐twisted walls about 0.3 μm in diameter. Exuvia cannot be distinguished from the exoskeletons of dead animals. The exoskeletal ultrastructure in trilobites agrees essentially with that in crust
展开▼