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Crystallography of surface precipitates associated with shape change in a Ti-5.26 wt. Cr alloy

机译:Ti-5.26 wt. Cr合金中与形状变化相关的表面析出物的晶体学

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摘要

The crystallographic features of surface α precipitates accompanied by surface tilt(s) in a Ti-5.26 wt. Cr alloy have been comprehensively studied by transmission electron microscopy of samples prepared using a focused ion beam. For comparison, the bulk precipitates formed far below the free surface in the same alloy have also been examined. It is found that both the surface and the bulk ot precipitates exhibit a lath-shaped morphology and their habit plane always contains a single set of misfit dislocations with the Burgers vector 1 1 l_β/22 11 3_α/6. However, the surface precipitates differ from the bulk ones in terms of their orientation relationship with the matrix, the habit plane and the long axis direction. As a result, the interphase interface between the surface precipitates and matrix contains glissile dislocations and the interface of bulk precipitates is associated with sessile dislocations. Such a glissile interface is one of the major common features of displacive-diflfusional and martensitic transformations and can be used to further understand the mechanism of bainitic transformation in steels and other alloy systems.
机译:通过聚焦离子束制备的样品的透射电子显微镜,对Ti-5.26 wt.%Cr合金中表面α析出物伴有表面倾斜的晶体学特征进行了全面研究。为了进行比较,还检查了在同一合金中远低于自由表面形成的块状沉淀物。结果表明,表面和块状沉淀物均呈现板条形貌,其习性平面始终包含一组错配位错,其Burgers向量为[1 1 l]_β/2|[2 11 3]_α/6.然而,表面析出物在与基体的取向关系、习性平面和长轴方向上与块状沉淀物不同。因此,表面析出物和基体之间的相界面包含滑行位错,而块状析出物的界面与无柄位错有关。这种滑行界面是位移-扩散和马氏体相变的主要共同特征之一,可用于进一步了解钢和其他合金体系中贝氏体相变的机理。

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