Simultaneous determination of clofentezine, fenoxycarb and hexythiazox by HPLC on apples, pears and their pulps

摘要

AbstractThe simultaneous HPLC determination of clofentezine, fenoxycarb and hexythiazox in apples, pears and their pulps is described. The method is based on a clean‐up procedure carried out on a Seppak C18 cartridge followed by HPLC analysis on an RP‐18 column using acetonitrile + water as mobile phase. Average recoveries were 85.0 for clofentezine, 84.8 for fenoxycarb and 75.6 for hexythiazox on apple matrix; recoveries from pear matrix were in the same range. UV detection limits at 240 nm were 0.07 mg kg−1for clofentezine, 0.064 mg kg−1for fenoxycarb and 0.08 mg kg−1for he