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Effect of thermal oxidation on helium implanted 316L stainless steel

机译:热氧化对氦气注入316L不锈钢的影响

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摘要

The effect of thermal oxide layer on He implanted 316L stainless steel was studied to evaluate experimentally how thermal oxidation affects the diffusion and distribution of He in the material. In the case of thermal oxidation of a He implanted sample, with an increase in oxidation time, the max swelling height increases logarithmically as a function of time and finally saturates for all samples except for the lowest dose of implanted He. Concerning TEM results, two void regions are identified. Similar to the calculation, the total irradiated depth was around 250 nm and the large void region was formed around 100-150 nm depth. On the other hand, the small void region was observed immediately under oxide layer from the thermal oxidation. In contrast, there were no voids in the altered zone near the metal/oxide interface in the non-thermal oxidized/He implanted sample. This description of the phenomena was justified using the Kirkendall effect and the Point Defect Model. Published under an exclusive license by AIP Publishing.
机译:研究了热氧化层对He植入316L不锈钢的影响,通过实验评估了热氧化对He在材料中的扩散和分布的影响。在氦气注入样品热氧化的情况下,随着氧化时间的增加,最大溶胀高度作为时间的函数对数增加,最终除最低剂量的氦气外,所有样品都达到饱和。关于TEM结果,确定了两个空隙区域。与计算类似,总照射深度约为250 nm,大空隙区域在100-150 nm深度附近形成。另一方面,在热氧化的氧化层下立即观察到小空隙区域。相比之下,在非热氧化/氦气注入样品中,金属/氧化物界面附近的蚀变区域没有空隙。这种现象的描述是用Kirkendall效应和点缺陷模型来证明的。在 AIP Publishing 的独家许可下发布。

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