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Enhanced response speed of SAW based hydrogen sensor employing a micro-heater

机译:采用微加热器的SAW氢气传感器的响应速度提高

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摘要

To feature fast hydrogen detection, a new design of surface acoustic wave (SAW) based hydrogen sensor integrated with a micro-heater is proposed in this paper. A 200 MHz delay-line patterned SAW sensing chip coated Pd/Ni alloy hydrogen sensitive film and a micro-heater are prepared on a Y35oX quartz wafer. The hydrogen gas adsorption in Pd/Ni thin-film modulates the SAW propagation, and against the temperature interference, the corresponding changes in acoustic attenuation are collected as the sensor signal. The Micro-heater is designed to catalysis the gas-sensitive effect by regulating the working temperature, and the influence law of heating temperature towards response speed is revealed theoretically, allowing determination of the optimal working temperature. The experimental results verify the theoretical prediction. Fast response (t90 < 2 s), lower power consumption (<1.35 W), and the low detection limit (<15 ppm) are achieved at low working temperature of 75 degrees C. Furthermore, very low crossed humidity sensitivity and excellent long-term stability are observed. (c) 2023 Hydrogen Energy Publications LLC. Published by Elsevier Ltd. All rights reserved.
机译:为了实现快速氢气检测,该文提出了一种集成了微加热器的表面声波(SAW)氢气传感器的新设计。在Y35oX石英晶片上制备了200 MHz延迟线图案化的SAW传感芯片包覆Pd/Ni合金氢敏膜和微加热器。Pd/Ni薄膜中的氢气吸附调制了SAW的传播,并针对温度干扰,将相应的声衰减变化收集为传感器信号。微型加热器通过调节工作温度来催化气敏效应,从理论上揭示了加热温度对响应速度的影响规律,从而确定了最佳工作温度。实验结果验证了理论预测的正确性。在75°C的低工作温度下,实现了快速响应(t90<2 s)、低功耗(<1.35 W)和低检出限(<15 ppm)。此外,还观察到非常低的交叉湿度敏感性和出色的长期稳定性。(c) 2023 Hydrogen Energy Publications LLC.,由Elsevier Ltd.出版。保留所有权利。

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