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Surface tension of liquid Fe, Nb and 304L SS and effect of drop mass in aerodynamic levitation

机译:液态Fe、Nb和304L SS的表面张力及气动悬浮中液滴质量的影响

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摘要

The oscillating drop method has been widely used for surface tension measurements of liquids at high temperatures such as molten metals. An experimental device that permits such measurements has been developed at IRDL. This device relies on aerodynamic levitation for the sample to be contactless and on acoustic excitation to make it oscillate at its resonance frequency, which is related to the surface tension with Rayleigh's equation. Beforehand, experimentally, a lateral gas jet blows and controls the rotation of the drop due to its unpredictable behavior. Moreover, the effect of drop mass, usually studied for electromagnetic levitation, remains unknown for aerodynamic levitation. To fill this knowledge gap, levitated drops of different masses were numerically modeled to observe the influence of gravity or additional oscillation modes. It resulted that for light mass drops, such as those used for our surface tension measurement, it is not significant. Finally, our results on iron, niobium, and 304L stainless steel have been compared with the literature. For pure metals, we observed a similar decreasing behavior versus temperature. For steel, results highlighted the impact of experimental parameters on the surface tension (length of experiments and composition of the atmosphere). These measurements thus provide original results that will be useful for the numerical modeling of innovative industrial processes such as additive manufacturing or welding.
机译:振荡液滴法已广泛用于高温液体(如熔融金属)的表面张力测量。IRDL已经开发了一种允许进行此类测量的实验设备。该装置依靠空气动力学悬浮使样品实现非接触式,并依靠声激励使其在其共振频率下振荡,这与瑞利方程的表面张力有关。事先,通过实验,由于其不可预测的行为,横向气体射流吹气并控制液滴的旋转。此外,通常针对电磁悬浮进行研究的液滴质量的影响对于空气动力学悬浮仍然未知。为了填补这一知识空白,对不同质量的悬浮液滴进行了数值建模,以观察重力或其他振荡模式的影响。结果,对于轻质量液滴,例如用于表面张力测量的液滴,它并不显着。最后,将铁、铌和304L不锈钢的结果与文献进行了比较。对于纯金属,我们观察到类似的随温度下降的行为。对于钢,结果突出了实验参数对表面张力(实验长度和大气成分)的影响。因此,这些测量提供了原始结果,可用于创新工业过程(如增材制造或焊接)的数值建模。

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