首页> 外文期刊>Mapan: Journal of Metrology Society of India >Development of Nickel-Carbon Eutectic Fixed Point Cell for Thermocouple Thermometry
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Development of Nickel-Carbon Eutectic Fixed Point Cell for Thermocouple Thermometry

机译:用于热电偶测温的镍碳共晶定点电池的开发

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摘要

The novel materials of different phase transition temperatures are exploited in thermometry as defined fixed points to form the International Temperature Scales (ITS). In the high-temperature range above the copper fixed point (1084.62 degrees C), melting transition temperatures of metal-carbon (M-C) eutectics are evolved as reference fixed points to disseminate T-90 and thermodynamic temperature (T). This paper presents the development and realization parameters of Ni-C eutectic fixed point cells for thermocouple thermometry. These cells are successfully fabricated using a single (NPLI Ni-C-01) and multiple filling (NPLI Ni-C-02) approaches, and optimization of various parameters such as repeatability of melting and freezing, long-term stability, heat-flux effect, and cell realization uncertainty are reported. The assigned temperatures to single and multiple-filled fixed point cells using Type-S-TC are 1328.29 degrees C +/- 0.59 degrees C and 1328.46 degrees C +/- 0.59 degrees C, respectively. The results obtained for in-house developed NPLI Ni-C cells are in excellent agreement with the other NMIs and will support the assignment of temperature to Ni-C fixed point in future ITS.
机译:不同相变温度的新型材料在测温中作为定义的固定点进行利用,形成国际温标(ITS)。在铜固定点(1084.62°C)以上的高温范围内,金属-碳(M-C)共晶的熔融转变温度演变为参考不动点,以传播T-90和热力学温度(T)。本文介绍了用于热电偶测温的Ni-C共晶定点电池的发展和实现参数。采用单次(NPLI Ni-C-01)和多次填充(NPLI Ni-C-02)方法成功制备了这些电池,并报告了熔融和冷冻的重复性、长期稳定性、热通量效应和电池实现不确定性等各种参数的优化。使用 Type-S-TC 的单填充和多填充定点单元的分配温度分别为 1328.29 摄氏度 +/- 0.59 摄氏度和 1328.46 摄氏度 +/- 0.59 摄氏度。内部开发的NPLI镍-C电池的结果与其他NMIs非常吻合,并将支持未来ITS中Ni-C固定点的温度分配。

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