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In‐situdeactivation of packed columns for SFC

机译:SFC填充柱的In-situde激活

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AbstractResidual adsorptive activity of reversed phase (RP) column packings used in supercritical fluid chromatography (SFC) can be significantly reduced by a dynamicin‐situsilanization with diphenyltetramethyldisilazane (DPTMDS). RP‐materials thus deactivated were characterized both chromatographically and by solid‐phase29S
机译:摘要超临界流体色谱(SFC)中反相(RP)柱填料的残余吸附活性可通过二苯基四甲基二硅氮烷(DPTMDS)进行动态原位硅烷化反应显著降低。通过色谱和固相29S对失活的RP材料进行了表征

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