首页> 外文期刊>Journal of Rubber Research >Effect of silanised reinforcements on thermal, wear, visco-elastic and fatigue behaviour of stitched E-glass fibre-reinforced epoxy hybrid composite
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Effect of silanised reinforcements on thermal, wear, visco-elastic and fatigue behaviour of stitched E-glass fibre-reinforced epoxy hybrid composite

机译:硅烷化增强对缝合E-玻璃纤维增强环氧杂化复合材料热,磨损,粘弹性和疲劳行为的影响

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Carboxyl-terminated butadiene acrylonitrile liquid rubber toughened silicon carbide and stitched E-glass fibre-reinforced epoxy composite has been fabricated and tested for their relative effect on thermal, wear, visco-elastic and fatigue behaviour. The main objective of this present work is to explicate the importance of rubber toughening on high brittle polymer matrix and the need for secondary strengthening to improve properties. The reinforcements were surface-treated using an amine-functional coupling agent for better adhesion and uniform dispersion on matrix. The composites were made using hand layup method and post cured at 120 degrees C. The addition of micro rubber into epoxy resin improved the fatigue and visco-elastic properties with a marginal decrement in thermal stability and wear resistance behaviour whereas the addition of silicon carbide significantly improved the properties. A highest fatigue life cycle of 12,941 and storage modulus of 7.8 GPa was observed for composite contains 1 and 10 vol% of silicon carbide and micro rubber, respectively. The initial thermal stability of composite, which contains 2 and 10 vol% of reinforcement measures 348 degrees C and the lowest coefficient of friction of 0.36 and specific wear rate of 0.028 mm(3)/Nm. The Scanning electron microscope images illustrate uniform dispersion and improved adhesion of silane surface-modified reinforcements in epoxy matrix. These high toughness polymer composites could be used in high load-bearing engineering applications wherever possible.
机译:制备了端羧基丁二烯-丙烯腈液体橡胶增韧碳化硅和缝合E-玻璃纤维增强环氧树脂复合材料,并测试了它们对热、磨损、粘弹性和疲劳性能的相对影响。本研究的主要目的是阐明橡胶在高脆性聚合物基体上增韧的重要性,以及二次强化以改善性能的必要性。使用胺功能偶联剂对增强体进行表面处理,以获得更好的附着力和在基体上的均匀分散。复合材料采用手糊法制成,并在120℃下后固化。在环氧树脂中添加微橡胶可改善疲劳和粘弹性性能,热稳定性和耐磨性略有下降,而添加碳化硅可显著改善性能。对于碳化硅和微橡胶含量分别为1%和10%的复合材料,其最高疲劳寿命为12941,储能模量为7.8 GPa。复合材料的初始热稳定性(含2%和10%的增强体)为348℃,最低摩擦系数为0.36,比磨损率为0.028 mm(3)/Nm。扫描电镜图像显示,硅烷表面改性增强体在环氧树脂基体中均匀分散,附着力提高。这些高韧性聚合物复合材料可以在任何可能的情况下用于高承载工程应用。

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