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Green Synthesis of Silver Nanoparticles by Using Ziziphus nummularia Leaves Aqueous Extract and Their Biological Activities

机译:使用Ziziphus Nummularia留下含水提取物及其生物活性的银纳米粒子的绿色合成

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摘要

Silver nanoparticles of Ziziphus nummularia leaves extract were synthesized and were characterized by UV-Visible spectrophotometry, particle size analyzer, X-ray diffraction (XRD), differential scanning calorimetry (DSC), Fourier transform infrared spectroscopy (FT-IR), SEM, TGA, and EDX. The XRD pattern reveals the FCC structure of Ag nanoparticles. FTIR spectra confirmed the presence of Ag-O bonding. UV-Visible spectroscopy results confirmed the existence of Ag because of the particular peak in the region of 400-430. The SEM analysis confirmed spherical and uniform Ag nanoparticles with diameter ranging from 30nm to 85 nm. The EDX analysis revealed strong signals in the silver region and confirmed the formation of silver nanoparticles. The antioxidant potential and antifungal and antimicrobial potential of the leaf extract and silver nanoparticles were also determined. The antioxidant property was determined using DPPH assay. The antibacterial, antifungal, and antioxidant properties were better for the silver nanoparticles than the aqueous leaf extract. The minimum inhibitory concentration (MIC), minimum bactericidal (MBC), and minimum fungicidal concentration (MFC) of plant extract and prepared silver nanoparticles were also tested. The hair growth properties of plant extracts and their respective nanoparticles were observed and good results were noted for nanoparticles as compared to the leaf extract.
机译:合成了红枣叶提取物中的银纳米粒子,并用紫外可见分光光度法、粒度分析仪、X射线衍射(XRD)、差示扫描量热法(DSC)、傅立叶变换红外光谱(FT-IR)、扫描电镜(SEM)、热重分析(TGA)和能谱仪(EDX)对其进行了表征。XRD图谱显示了银纳米颗粒的FCC结构。FTIR光谱证实了银氧键的存在。紫外-可见光谱结果证实了银的存在,因为在400-430区域有一个特殊的峰。SEM分析证实,银纳米颗粒呈球形且均匀,直径在30nm至85nm之间。EDX分析揭示了银区域的强信号,并证实了银纳米颗粒的形成。还测定了叶提取物和银纳米颗粒的抗氧化潜力、抗真菌和抗菌潜力。采用DPPH法测定抗氧化性能。银纳米颗粒的抗菌、抗真菌和抗氧化性能优于水叶提取物。还测试了植物提取物和制备的银纳米颗粒的最小抑菌浓度(MIC)、最小杀菌浓度(MBC)和最小杀菌浓度(MFC)。观察了植物提取物及其各自纳米颗粒的毛发生长特性,发现纳米颗粒与叶提取物相比效果良好。

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