Thermomechanical analysis of the crack tip zone in stretched crystallizable natural rubber by using infrared thermography and digital image correlation

摘要

This paper provides the first characterization of heat source field in the crack tip zone in carbon black filled natural rubber (NR). It focuses more especially on the calorific effects of strain induced. crystallization (SIC). For this purpose, full thermal and kinematic fields are measured simultaneously. Initial image processing based on motion compensation enables us to track the temperature of any material point at the specimen surface. A second image processing stage, based on the heat diffusion equation, enables us to obtain the fields of heat sources produced and absorbed by the material during the test. The heterogeneity of the stretch states is analyzed from the kinematic measurements. In terms of heat production, crystallization acts in two opposite ways in the crack tip zone: the crystallization process produces additional heat, but crystallites act as fillers, which increases material stiffness in the crack tip zone. Moreover, the heat sources in the crack tip zone remain positive and small during unloading. This phenomenon is due to the production of mechanical dissipation and probably a continuation of the crystallization process. The results attained are compared with those recently obtained in non-crystallizing carbon black filled styrene butadiene rubber (SBR50). (C) 2014 Elsevier Ltd. All rights reserved.