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Flash microwave synthesis of trevorite nanoparticles

机译:闪速微波合成水合纳米粒子

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Nickel ferrite nanoparticles have several possible applications as cathode materials for rechargeable batteries, named "lithium-ion" batteries. In this study, NiFe2O4 was prepared by microwave induced thermohydrolysis. The obtained nanoparticles were characterized by scanning electron microscopy (SEM) and energy dispersive X-ray spectroscopy (EDX), X-ray diffraction (XRD), BET method, transmission electron microscopy (TEM) and small angle X-ray scattering (SAXS). All the results show that the microwave one-step flash synthesis leads in a very short time to NiFe2O4 nanoparticles with elementary particles size close to 4-5 nm, and high specific surfaces (close to 240 m(2)/g). Thus, microwave heating appears as an efficient source of energy to produce quickly nanoparticles with complex composition as ferrite. (C) 2008 Elsevier Inc. All rights reserved.
机译:镍铁氧体纳米粒子有几种可能的应用,它们被称为可再充电电池的正极材料,称为“锂离子”电池。在这项研究中,NiFe2O4是通过微波诱导的热水解制备的。通过扫描电子显微镜(SEM)和能量色散X射线光谱(EDX),X射线衍射(XRD),BET法,透射电子显微镜(TEM)和小角X射线散射(SAXS)对获得的纳米颗粒进行表征。所有结果表明,微波一步快速合成法在很短的时间内导致了NiFe2O4纳米粒子的基本粒径接近4-5 nm,并且具有高比表面积(接近240 m(2)/ g)。因此,微波加热似乎是快速生产具有复杂组成的铁氧体纳米粒子的有效能源。 (C)2008 Elsevier Inc.保留所有权利。

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