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Determination of Cr(VI) concentration in diluted samples based on the paper test strip method

机译:纸试纸法测定稀释样品中的六价铬

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摘要

At present, there are many methods for Cr(VI) concentration determination in diluted samples,nhowever, these methods have their own inherent drawbacks, such as long response time,ncomplicated pretreatment, expensive equipment etc. In this paper, a paper-based test strip methodnspecific for determination of diluted Cr(VI) samples was developed. In this method, Aliquat 336, asnan anion exchanger was loaded into filter paper to form a test strip. This test strip was used to pre-nconcentrate Cr(VI) when contacting with the diluted Cr(VI)-containing solution. The Cr(VI)-containingntest strip was then immersed into a diphenylcarbazide (DPC) solution (a color forming solution), andnthe color intensity was correlated to the Cr(VI) concentration. The detection range of the presentnmethod was found to be 0.02–1.50mg/L. The results also showed that the method gave a highnselectivity for Cr(VI) in the diluted samples to be tested. The method was applied to synthesizednsamples and the results, which were compared to those from a reference method, showed thatnthe developed method is an effective, reliable way for Cr(VI) determination in diluted samples.
机译:目前,用于稀释样品中Cr(VI)浓度测定的方法很多,但是这些方法都有其固有的缺点,如响应时间长,预处理复杂,设备昂贵等。开发了专门用于测定稀释的Cr(VI)样品的检测方法。在这种方法中,将亚砜阴离子交换剂Aliquat 336装入滤纸中以形成测试条。当与稀释的含Cr(VI)溶液接触时,该试纸条用于预浓缩Cr(VI)。然后将含Cr(VI)的测试条浸入二苯卡巴肼(DPC)溶液(成色溶液)中,然后将颜色强度与Cr(VI)浓度相关。本方法的检测范围为0.02-1.50mg / L。结果还表明,该方法对待测稀释样品中的Cr(VI)具有较高的选择性。该方法应用于合成样品,并与参考方法进行比较,结果表明,该方法是测定稀释样品中Cr(VI)的有效,可靠方法。

著录项

  • 来源
    《Water Science and Technology》 |2009年第12期|p.3083-3089|共7页
  • 作者

    F. Kong and Y. Ni;

  • 作者单位

    F. KongKey Laboratory of Pulp and Paper Engineering ofEducation Ministry of China,Shandong Institute of Light Industry,Jinan 250353,ChinaE-mail: kfgwsj1566@163.comY. NiLimerick Pulp and Paper Centre,University of New Brunswick,Fredericton E3B 6C2, New Brunswick,CanadaE-mail: yonghao@unb.ca;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    chromium (VI), diluted samples, diphenylcarbazide, test strip method;

    机译:六价铬;稀释样品;二苯卡巴肼;试纸条法;

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