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One-pot synthesis of α-Fe_2O_3 nanoparticles-decorated reduced graphene oxide for efficient nonenzymatic H_2O_2 biosensor

机译:一锅合成α-Fe_2O_3纳米粒子修饰的还原氧化石墨烯,用于高效非酶H_2O_2生物传感器

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摘要

Hematite nanoparticles (α-Fe_2O_3) are successfully decorated on the reduced graphene oxide (rGO) sheets through a simple, one-step, hydrothermal method without addition of other reducing agents. The α-Fe_2O_3/rGO hybrid was characterized by scanning electron micrographs, X-ray diffraction, X-ray photo-electron spectroscopy, and Raman spectroscopy. This α-Fe_2O_3/rGO hybrid has been successfully applied in the catalytic performance toward the reduction of H_2O_2. The nonenzymatic sensor demonstrates a linear relationship over a wide concentration range of 5.0-4495.0 μM (R=0.9998), a low detection limit of 1.0 μM, and a high sensitivity of 126.9 μAcm~(-2)mM~(-1) to the detection of H_2O_2.
机译:通过简单的一步式水热方法,无需添加其他还原剂,即可在还原的氧化石墨烯(rGO)板上成功修饰赤铁矿纳米粒子(α-Fe_2O_3)。通过扫描电子显微镜,X射线衍射,X射线光电子能谱和拉曼光谱来表征α-Fe_2O_3/ rGO杂化物。该α-Fe_2O_3/ rGO杂化体已成功地用于催化性能,以还原H_2O_2。该非酶传感器在5.0-4495.0μM(R = 0.9998)的宽浓度范围,1.0μM的低检测限和126.9μAcm〜(-2)mM〜(-1)的高灵敏度范围内表现出线性关系。 H_2O_2的检测。

著录项

  • 来源
    《Sensors and Actuators》 |2014年第1期|645-650|共6页
  • 作者单位

    Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang, 222005, China,Intelligent Polymer Research Institute, ARC Centre of Excellence for Electromaterials Science, Australian Institute of Innovative Materials, University of Wollongong, Northfields Avenue, Wollongong, NSW 2522, Australia;

    Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang, 222005, China;

    Intelligent Polymer Research Institute, ARC Centre of Excellence for Electromaterials Science, Australian Institute of Innovative Materials, University of Wollongong, Northfields Avenue, Wollongong, NSW 2522, Australia;

    Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang, 222005, China;

    Department of Chemical Engineering, Huaihai Institute of Technology, Lianyungang, 222005, China;

    Intelligent Polymer Research Institute, ARC Centre of Excellence for Electromaterials Science, Australian Institute of Innovative Materials, University of Wollongong, Northfields Avenue, Wollongong, NSW 2522, Australia;

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  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    α-Fe_2O_3 nanoparticles; Reduced graphene oxide; Nonenzymatic; Sensor;

    机译:α-Fe_2O_3纳米粒子;氧化石墨烯还原;非酶传感器;

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