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Production of cyclo-hafnium metal-organic thin film using a specific method

机译:使用特定方法生产环-金属有机薄膜

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摘要

Cyclo-hafnium metal-organic thin film was successfully synthesized and deposited on amorphous glass using a specific method, where amorphous substrate was used for synthesis and coating. Then, the film was annealed at 300 degrees C in an oven (ambient conditions). Optical and structural properties of the films were also investigated within the study. The structure of the film was analyzed using the mid-infrared spectrum. Optical properties were investigated via the UV-Vis spectroscopic technique. Film thickness was measured with AFM (tapping mode). Surface properties and elemental ratio of the films were examined and measured with SEM and EDX analysis. The highest transmittance and lowest reflectance values within the visible range were identified. The characteristic triethanolamine and hafnium-oxide peaks were observed in the infrared spectrum. FIR spectra of the films were found to be in accordance with the literature. SEM images of the films revealed that the surface of the films is fragile. EDX analysis of hafnium, organic parts of the compound and some minerals of amorphous glass were shown.
机译:成功地合成了环-金属有机薄膜,并使用一种特定方法将其沉积在非晶玻璃上,其中使用非晶衬底进行合成和涂覆。然后,将膜在烘箱中(环境条件)在300℃下退火。在研究中还研究了薄膜的光学和结构性质。使用中红外光谱分析膜的结构。通过UV-Vis光谱技术研究了光学性质。膜厚用AFM(拍击模式)测量。通过SEM和EDX分析检查并测量了膜的表面性质和元素比。确定了可见范围内的最高透射率和最低反射率值。在红外光谱中观察到特征性的三乙醇胺和氧化ha峰。发现该膜的FIR光谱与文献一致。膜的SEM图像显示出膜的表面易碎。对DX,化合物的有机部分和非晶玻璃的某些矿物进行了EDX分析。

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