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首页> 外文期刊>Nuclear Instruments & Methods in Physics Research >A novel room temperature-induced chemical etching (RTCE) technique for the enlargement of fission tracks in Lexan polycarbonate SSNTD
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A novel room temperature-induced chemical etching (RTCE) technique for the enlargement of fission tracks in Lexan polycarbonate SSNTD

机译:一种新的室温诱导化学蚀刻(RTCE)技术,用于扩大Lexan聚碳酸酯SSNTD中的裂变径迹

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The chemical or electrochemical etching is an essential step to enlarge the ion-induced latent tracks in solid state nuclear track detectors (SSNTDs). In these methods, above ambient temperatures (~60 ℃) and moderately high concentrations of alkali are required for about 1-2 h to enlarge the latent tracks. Microwave induced chemical etching method is reported to reduce the etching time for alpha tracks from 3 to 4 h to 25 min for CR-39 detector. In the present work, a room temperature-induced chemical etching employing ethanolamine as a new etchant has been investigated for the first time to enlarge the fission tracks in Lexan polycarbonate SSNTD. The tracks developed in the Lexan detectors etched at room temperature using ethanolamine are compared with those etched with routinely used chemical etching (CE) technique in 6 N NaOH at 60 ℃. The bulk etch and track etch rates are also reported. The detection efficiency of RTCE method is determined and compared with that of CE method. The RTCE technique is found to be simple, fast and convenient.
机译:化学或电化学蚀刻是在固态核径迹检测器(SSNTD)中扩大离子感应潜迹的必不可少的步骤。在这些方法中,需要超过环境温度(〜60℃)和适度高浓度的碱约1-2小时,以扩大潜迹。据报道,微波诱导化学刻蚀方法可将CR-39检测器的α迹线刻蚀时间从3到4 h减少到25 min。在目前的工作中,首次研究了使用乙醇胺作为新蚀刻剂的室温诱导化学蚀刻,以扩大Lexan聚碳酸酯SSNTD中的裂变径迹。将在Lexan检测器中室温下使用乙醇胺蚀刻的轨迹与在60 N的6 N NaOH中使用常规化学蚀刻(CE)技术蚀刻的轨迹进行比较。还报告了体蚀刻和轨迹蚀刻速率。确定了RTCE方法的检测效率,并与CE方法进行了比较。发现RTCE技术是简单,快速和方便的。

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