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Hot-deformation behaviour of spray-formed 2014 Al + SiCp metal matrix composites

机译:喷射成型2014 Al + SiCp金属基复合材料的热变形行为

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In the present investigation, discontinuous SiC particle reinforced 2014 Al alloy based metal matrix composites have been produced by spray forming process. The composites contained average particle sizes of 17, 30 and 58 μm in the range of 5-11 vol.%. The composites were tested for their compressive flow behaviour, in unlubricated condition, at strain rates of 0.01, 0.1 and 1.0 s~(-1) and at temperatures of 150, 300 and 450 ℃. The flow stress for 30 |xm size particle reinforced composite increased with increasing particle content from 0 to 8.5 vol.%, but decreased at 11 vol.%. The flow stress invariably decreased at larger strain values during deformation. The increase in particle size from 17 to 30 μm led to increase in flow stress at 300 ℃, whereas, it decreased at 450 ℃. The strain rate sensitivity (m) for 30 μm size particle reinforced composite was close to 0.16 up to 8.5 vol.%, whereas, for the composite with 17 μm size particles it decreased to 0.13 with increasing volume fraction up to 8.6 vol.%. The m values increased from 0.13 to 0.15 with increase in particle size from 17 to 58 μm. The variation in flow behaviour has been attributed mainly to particle fracture and debonding at particle/matrix interface, confirmed by microstructural features of the deformed samples. The major particle fracture events were recorded at low temperature and low strain rate of deformation. The composite with 30 μm size particles showed enhanced restoration process based on the low value of calculated apparent activation energy for diffusion (80-100 kJmol~(-1)). This deformation behaviour of the composites has been discussed in light of microstructural observations and the void formation during deformation.
机译:在本研究中,已经通过喷涂成型工艺生产了不连续的SiC颗粒增强的2014 Al合金基金属基复合材料。该复合材料的平均粒径为17、30和58μm,范围为5-11 vol。%。在未润滑条件下,应变率为0.01、0.1和1.0 s〜(-1)以及温度为150、300和450℃的条件下,测试了复合材料的压缩流动行为。 30 xm尺寸的颗粒增强复合材料的流动应力随着颗粒含量从0到8.5体积%的增加而增加,而在11体积%时降低。在变形过程中,在较大的应变值下,流动应力始终减小。粒径从17μm增加到30μm导致在300℃时流动应力增加,而在450℃时减小。 30μm尺寸的颗粒增强复合材料的应变速率灵敏度(m)接近0.16,最大为8.5 vol。%,而具有17μm尺寸的颗粒的复合材料的应变率灵敏度降低到0.13,而体积分数最大为8.6 vol。%。随着粒径从17微米增加到58微米,m值从0.13增加到0.15。流动行为的变化主要归因于颗粒破裂和在颗粒/基体界面处的脱粘,这由变形样品的微观结构特征证实。在低温和低应变变形率下记录了主要的颗粒破裂事件。粒径为30μm的复合材料由于计算出的表观扩散活化能较低(80-100 kJmol〜(-1)),因此恢复过程得到了增强。结合微观结构观察和变形过程中空隙的形成,已经讨论了复合材料的这种变形行为。

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