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Microstructure and mechanical properties of direct laser metal deposited Haynes 282 superalloy

机译:直接激光沉积金属Haynes 282高温合金的组织和力学性能

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Direct laser metal deposition (LMD) is a directed energy deposition based additive manufacturing process developed for a wide range of applications that are currently employed in aerospace, medical and automotive sectors. In the present study, a 100 mm x 15 mm x 25 mm block of Haynes 282 (HY282) superalloy was fabricated by LMD. The effect of several post-deposition heat-treatments revealed a wide range of strength and ductility of HY282 samples that can be tuned to obtain the best material properties. The microstructure and mechanical properties of the as-deposited and heat-treated specimens are investigated using scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS), X-ray-diffraction (XRD), uniaxial tension test, and micro-hardness measurements. The SEM and XRD investigation revealed the formation of columnar dendrites having [001] growth direction opposite to the heat flow direction during LMD. The as-deposited samples revealed the presence of gamma, gamma', Ti and Mo-rich MC, and Mo-rich M6C phases with the strengthening gamma' phase having an average precipitate size of 8.25 nm in the interdendritic region. The EDS investigation revealed the uniform distribution of Ni, Al, Cr, Co in the overall deposit with high segregation of Ti and Mo in the interdendritic regions. The corresponding hardness of 294 HV, yield strength of 633 MPa, and 31.5% elongation was recorded in the as-deposited samples that were better than the as-cast properties. The LMD specimen heat treated at 788 degrees C for 16 h revealed a homogeneous distribution of gamma' with an average size of 31 nm with a globular and Chinese script type carbides interconnected in the interdendritic region. The corresponding hardness of 410 HV, yield strength of 894 MPa, ultimate tensile strength of 1200 MPa, and 18% elongation was recorded. These results establish that HY282 is an attractive material for the LMD process.
机译:直接激光金属沉积(LMD)是一种基于定向能量沉积的增材制造工艺,专门针对航空航天,医疗和汽车领域目前广泛使用的应用而开发。在本研究中,LMD制造了100毫米x 15毫米x 25毫米的Haynes 282(HY282)超级合金块。几种沉积后热处理的效果表明,HY282样品具有广泛的强度和延展性,可以对其进行调整以获得最佳的材料性能。使用扫描电子显微镜(SEM),能量色散X射线光谱(EDS),X射线衍射(XRD),单轴拉伸试验和显微技术研究了沉积和热处理后的样品的微观结构和力学性能。硬度测量。 SEM和XRD研究表明,形成了具有与LMD过程中的热流方向相反的[001]生长方向的柱状树枝状晶体。沉积样品显示存在γ,γ',富Ti和Mo的MC和富Mo的M6C相,强化的γ'相在树突间区域的平均析出尺寸为8.25 nm。 EDS调查显示,镍,铝,铬,钴在整个沉积物中分布均匀,而在枝晶间区域中钛和钼的高度偏析。在沉积后的样品中记录到相应的294 HV硬度,633 MPa的屈服强度和31.5%的伸长率,其性能优于铸造后的性能。在788℃热处理16 h的LMD试样显示出均匀分布的γ',平均尺寸为31 nm,球状和中文字型碳化物在树突区域相互连接。记录了相应的410 HV硬度,894 MPa的屈服强度,1200 MPa的极限拉伸强度和18%的伸长率。这些结果证明,HY282对LMD工艺具有吸引力。

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