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Screening of treated diatomaceous earth to apply as V_2O_5 catalyst support

机译:筛选处理过的硅藻土以用作V_2O_5催化剂载体

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In this study, we have modified the properties of diatomaceous earth precursors which are aimed to be used in the synthesis of V_2O_5 catalysts. Hence, in the first step, three various samples of Iranian diatomaceous earth were provided from Khorasan and East Azerbaijan mines. In the second step, V_2O_5 catalysts were synthesized with treated diatomite samples. In order to study the efficiency of acid treatment and the effect of diatomite precursors, characterization tests including XRD, ICP, BET-BJH, SEM and TEM were organized for each step. Eventually, results proved that acid treatment modified microstructure of some diatomaceous earth and increased the performance of the catalyst. The object of this research was to find the best treated diatomite support among Iranian mine and various conditions of acid treatment that can be used in commercial V_2O_5 catalyst. The results show that C15-Mi (catalyst with diatomite Mianeh mine treated with 15% acid concentration) has the best conversion among all samples.
机译:在这项研究中,我们修改了旨在用于V_2O_5催化剂合成的硅藻土前体的性能。因此,在第一步中,从霍拉桑和东阿塞拜疆矿场提供了三种不同的伊朗硅藻土样品。第二步,用处理过的硅藻土样品合成V_2O_5催化剂。为了研究酸处理的效率和硅藻土前体的影响,针对每个步骤组织了包括XRD,ICP,BET-BJH,SEM和TEM在内的表征测试。最终,结果证明了酸处理改变了某些硅藻土的微观结构并提高了催化剂的性能。这项研究的目的是在伊朗矿山中找到最佳处理的硅藻土载体,并在各种酸处理条件下找到可用于商业V_2O_5催化剂的硅藻土载体。结果表明,在所有样品中,C15-Mi(含硅藻土Mianeh矿的酸浓度为15%的催化剂)的转化率最高。

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