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Preparation of ZrB_2 based composites by reactive melt infiltration at relative low temperature

机译:较低温度下反应性熔体渗透制备ZrB_2基复合材料

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摘要

ZrB_2 based composites were prepared by a novel reactive melt infiltration process. The porous boron bars were used as preforms and infiltrated by the low melting Zr_2Cu intermetallic compound. Thermodynamics calculations revealed that B could react with liquid Zr_2Cu to form ZrB_2 as low as 1100 °C. Composites were prepared by heating the two materials to 1200 °C for 3 h in vacuum. The resultant composites were studied with XRD and SEM. ZrB_2 was identified to be the main constituent. The composites had a flexural strength of 414.3 MPa, a flexural modulus of 183.6 GPa, and a fracture toughness of 5.5 MPa m~(1/2).
机译:ZrB_2基复合材料是通过新型反应性熔体渗透工艺制备的。多孔硼棒用作预成型坯,并通过低熔点Zr_2Cu金属间化合物渗透。热力学计算表明,硼可以与液态Zr_2Cu反应形成低至1100°C的ZrB_2。通过将两种材料在真空中加热到1200°C 3 h来制备复合材料。用XRD和SEM研究所得的复合材料。 ZrB_2被确定为主要成分。该复合材料的弯曲强度为414.3 MPa,弯曲模量为183.6 GPa,断裂韧性为5.5 MPa m〜(1/2)。

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  • 来源
    《Materials Letters》 |2011年第20期|p.2910-2912|共3页
  • 作者单位

    Key Lab of Advanced Ceramic Fibres fXomposites, College of Aerospace ^Materials Engineering, National University of Defense Technology, Ckangsha 410073. PR China;

    Key Lab of Advanced Ceramic Fibres fXomposites, College of Aerospace ^Materials Engineering, National University of Defense Technology, Ckangsha 410073. PR China;

    Key Lab of Advanced Ceramic Fibres fXomposites, College of Aerospace ^Materials Engineering, National University of Defense Technology, Ckangsha 410073. PR China;

    Key Lab of Advanced Ceramic Fibres fXomposites, College of Aerospace ^Materials Engineering, National University of Defense Technology, Ckangsha 410073. PR China;

    Key Lab of Advanced Ceramic Fibres fXomposites, College of Aerospace ^Materials Engineering, National University of Defense Technology, Ckangsha 410073. PR China;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    ultra high temperature ceramics; intermetallic alloys and compounds; zirconium diboride; reactive melt infiltration;

    机译:超高温陶瓷;金属间合金和化合物;二硼化锆;反应熔体渗透;

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