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Facile synthesis of Fe3O4 nanowires at low temperature (80 degrees C) without autoclaves and their electromagnetic performance

机译:Fe3O4纳米线在没有高压釜的情况下在低温(80摄氏度)下轻松合成及其电磁性能

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摘要

Facile oxidation-precipitation processes were designed to produce high-quality Fe3O4 nanowires at 80 degrees C in an oxygen-free environment without autoclaves. Polyethyleneglycol (PEG) was used as soft template in synthesis procedures to regulate the single-crystal growth of Fe3O4 along [110] direction. The as-prepared Fe3O4 nanowires were characterized to be spinel structure with diameters in the range of 580 nm and lengths up to several micrometers. Their saturation magnetization and coercivity were examined to be 74.6 A.m(2).kg(-1) and 6471.5 A.m(-1) respectively. A maximum microwave absorption of -29.7 dB around 7.3 GHz was obtained as the Fe3O4 nanowires/paraffin composites were modulated in the thickness of 3.5 mm. (C) 2017 Elsevier B.V. All rights reserved.
机译:设计了简便的氧化沉淀工艺,可在无高压釜的无氧环境中于80摄氏度下生产高质量的Fe3O4纳米线。在合成程序中,使用聚乙二醇(PEG)作为软模板来调节Fe3O4沿[110]方向的单晶生长。所制备的Fe 3 O 4纳米线被表征为尖晶石结构,其直径在580nm的范围内并且长度高达数微米。他们的饱和磁化强度和矫顽力分别为74.6 A.m(2).kg(-1)和6471.5 A.m(-1)。当Fe3O4纳米线/石蜡复合材料的厚度调节为3.5 mm时,在7.3 GHz处可获得-29.7 dB的最大微波吸收。 (C)2017 Elsevier B.V.保留所有权利。

著录项

  • 来源
    《Materials Letters》 |2017年第15期|48-51|共4页
  • 作者单位

    China Univ Min & Technol, Sch Mat Sci & Engn, Xuzhou 221116, Peoples R China;

    China Univ Min & Technol, Sch Mat Sci & Engn, Xuzhou 221116, Peoples R China;

    China Univ Min & Technol, Sch Mat Sci & Engn, Xuzhou 221116, Peoples R China;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Magnetic materials; Fe3O4 nanowires; Microstructure; Microwave absorption;

    机译:磁性材料;Fe3O4纳米线;微观结构;微波吸收;

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