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Influence of heat treatment on anisotropic creep behavior of aluminide coating on a Ni-base single crystal superalloy

机译:热处理对镍基单晶高温合金上铝化物涂层各向异性蠕变行为的影响

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The influence of heat treatment on creep behavior of aluminide coating on a Ni-base single crystal super-alloy with different surface orientations was examined. The specimens were coated by pack aluminizing treatment at 1000 ℃ for 5 h under argon environment. The coated specimens were then tested by the tensile creep test at a temperature of 900 ℃ and a stress of 320 MPa. To determine the effect of aluminide coating, the bare specimens were also tested. The aluminizing treatment decreased the creep strength of Ni-base single crystal superalloy. The solution heat treatment procedures had a great impact on the creep behavior of Ni-base single crystal superalloy. The combination of solution treatment and subsequent double aging treatment was effective to improve the creep strength of Ni-base single crystal superalloy because of more regular the shape of γ' precipitates and more homogeneous distribution of γ' precipitates. In addition, the {100} specimens showed a better creep lives than those {110} specimens both in aluminized specimens and bare specimens. The anisotropic creep behavior was primarily induced by the different arrangement of {111} (101) slip systems between the two surface orientations of the specimens. The difference in creep rupture lives between {100} and {110} side-surface specimens was more pronounced in the specimens STA than in the specimens A because of homogenization of the γ/ γ' microstructure promoted the deformation by {111} (101) slip system which leads to anisotropy of creep behavior. Moreover, the change in microstructures was also considered as one of factors for the decrease of creep life. Besides, the formation of TCP phase, the depth of TCP phase penetration and the gradient of hardness values in the coating to the substrate regions would be additional factors to clarify the anisotropic creep behavior in aluminized Ni-base single crystal superalloy.
机译:研究了热处理对不同表面取向的镍基单晶高温合金上铝化物涂层蠕变行为的影响。在氩气环境下,在1000℃下进行渗铝处理,对试样进行5 h涂层。然后在900℃的温度和320 MPa的应力下通过拉伸蠕变测试对涂层样品进行测试。为了确定铝化物涂层的效果,还对裸露的样品进行了测试。渗铝处理降低了镍基单晶高温合金的蠕变强度。固溶热处理工艺对Ni基单晶高温合金的蠕变行为有很大影响。固溶处理和随后的双重时效处理的组合有效地提高了镍基单晶高温合金的蠕变强度,因为γ'沉淀的形状更规则并且γ'沉淀的分布更均匀。另外,在镀铝试样和裸露试样中,{100}试样的蠕变寿命都比{110}试样的蠕变寿命长。各向异性蠕变行为主要是由试样的两个表面方向之间的{111}(101)滑移系统的不同布置引起的。 {100}和{110}侧面试样之间的蠕变断裂寿命差异在试样STA中比在试样A中更为明显,这是因为γ/γ'微结构的均质化促进了{111}的变形(101)滑移系统,导致蠕变行为的各向异性。此外,微观结构的变化也被认为是降低蠕变寿命的因素之一。此外,TCP相的形成,TCP相渗透的深度以及涂层至基体区域的硬度值的梯度将是阐明铝化镍基单晶高温合金各向异性蠕变行为的附加因素。

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