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Preparation and Characterization of Properties of Microcapsules for Polymeric Composites Self-repairing

机译:高分子复合材料自修复微胶囊的制备及性能表征

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摘要

Microcapsules self-repairing polymeric composites belong to a new kind of smart materials. In this work, microcapsules used for polymeric composites self-repairing were prepared by in-situ polymerization. Optical microscopy, scanning electronic microscopy (SEM), fourier transfer infrared spectroscopy (FT-IR), and thermal gravity analysis (TGA) were used to determine the properties of prepared microcapsules such as grain size and their distribution, wall thickness, content of core materials and thermal performances of microcapsules. Results showed that the average grain size was 210 μm and the wall thickness was in the range of 1.8-5 μm depending on agitation rate. Thermal analysis indicated that the repairing agent's core materials were encapsulated in microcapsules.
机译:微胶囊自修复聚合物复合材料属于新型智能材料。在这项工作中,通过原位聚合制备用于聚合物复合材料自修复的微囊。使用光学显微镜,扫描电子显微镜(SEM),傅立叶转移红外光谱(FT-IR)和热重分析(TGA)来确定制备的微胶囊的性能,例如晶粒尺寸及其分布,壁厚,芯含量微胶囊的材料和热性能。结果表明,根据搅拌速率,平均晶粒尺寸为210μm,壁厚在1.8-5μm的范围内。热分析表明,修复剂的核心材料被封装在微胶囊中。

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