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Preparation and characterization of high photoactive TiO_2 catalyst using the UV irradiation-induced sol-gel method

机译:紫外辐照溶胶-凝胶法制备高光活性TiO_2催化剂及其表征

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High photoactive TiO_2 catalyst was prepared using the sol-gel method through UV irradiation during the formation stage of nuclei. The surface morphology and microstructure of the prepared catalyst were characterized using scanning electron microscopy (SEM), X-ray diffraction patterns (XRD), and Fourier transform infrared spectroscopy (FT-IR). The photoactivity was evaluated by the degradation of methylene blue. The results show that the photocatalysis of the prepared catalyst is higher than that of conventional heat-treated particles. The higher photoactivity is a combined result of favorable microstructure, appropriate hydroxyl groups, and active sites of Ti~(3+) ions on the surface of TiO_2. It is concluded that the ultraviolet irradiation-induced sol-gel method is an effective method to enhance the photocatalysis of TiO_2.
机译:在核形成阶段,采用溶胶-凝胶法通过紫外线辐照制备了高光活性TiO_2催化剂。用扫描电子显微镜(SEM),X射线衍射图谱(XRD)和傅里叶变换红外光谱(FT-IR)对制备的催化剂的表面形貌和微观结构进行表征。通过亚甲基蓝的降解来评价光活性。结果表明,所制备的催化剂的光催化性能高于常规的热处理颗粒。较高的光活性是良好的微观结构,适当的羟基和TiO_2表面上的Ti〜(3+)离子活性位点的综合结果。结论:紫外辐射诱导的溶胶-凝胶法是增强TiO_2光催化的有效方法。

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