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Evaluation of transient liquid phase bonding between nickel-based superalloys

机译:镍基高温合金之间瞬时液相键合的评估

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摘要

Induction brazing of Inconel 718 to Inconel X-750 using Ni-7Cr-3Fe-3.2B-4.5Si (wt.-%) foil as brazing filler metal was investigated in this paper. Brazing was conducted at the temperature range 1373–1473 K for 0–300 s in a flow argon environment. Both interfacial microstructures and mechanical properties of brazed joints were investigated to evaluate joint quality. The optical and scanning electron microscopic results indicate that good wetting existed between the brazing alloy and both Inconel 718 and Inconel X-750. Microstructures at joint interfaces of all samples show distinct multilayered structures that were mainly formed by isothermal solidification and following solid-state interdiffusion during joining. The diffusion of boron and silicon from brazing filler metal into base metal at the brazing temperature is the main controlling factor pertaining to the microstructural evolution of the joint interface. The element area distribution of Cr, Fe, Si, Ni and Ti was examined by energy dispersive X-ray analysis. It was found that silicon and chromium remain in the center of brazed region and form brittle eutectic phases; boron distribution is uniform across joint area as it readily diffuses from brazing filler metal into base metal. The influence of heating cycle on the microstructures of base material and holding time on the mechanical properties of brazed joint were also investigated.
机译:本文研究了使用Ni-7Cr-3Fe-3.2B-4.5Si(wt。%)箔片作为钎料将Inconel 718感应焊接到Inconel X-750的方法。在流动氩气环境中,在1373–1473 K的温度范围内进行钎焊0–300 s。研究了钎焊接头的界面微观结构和力学性能,以评估焊接质量。光学和扫描电子显微镜结果表明,钎焊合金与Inconel 718和Inconel X-750之间都具有良好的润湿性。所有样品的接合界面处的微结构均显示出明显的多层结构,这些结构主要是由等温凝固以及在接合过程中固态相互扩散形成的。硼和硅在钎焊温度下从钎料扩散到母材中的扩散是与接头界面的微观结构演变有关的主要控制因素。通过能量色散X射线分析检查了Cr,Fe,Si,Ni和Ti的元素面积分布。发现硅和铬保留在钎焊区域的中心并形成脆性的共晶相。硼在整个接缝区域均匀分布,因为它很容易从钎料扩散到贱金属中。还研究了加热周期对基体组织和保温时间对钎焊接头力学性能的影响。

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  • 来源
    《Journal of Materials Science》 |2001年第6期|1539-1546|共8页
  • 作者单位

    Division of Materials Engineering School of Applied Science Nanyang Technological University;

    Division of Materials Engineering School of Applied Science Nanyang Technological University;

    Division of Materials Engineering School of Applied Science Nanyang Technological University;

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  • 正文语种 eng
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