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A study on heat affected zone softening in resistance spot welded dual phase steel by nanoindentation

机译:纳米压痕法研究电阻点焊双相钢的热影响区软化

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摘要

The base metal (BM) and the heat affected zone (HAZ) of a resistance spot welded dual phase steel have been evaluated by nanoindentation hardness testing. Three different surface conditions have been explored on the BM for assessing the nanohardness response. Softening has been investigated along the sub-critical HAZ by making nanoindentations on individual phases such as ferrite and tempered martensite (TM) at various distances from the line of lower critical temperature Ac1. A broken appearance accompanied with sub-micron particles were consistently found on TM at 100 μm from the Ac1 line suggesting carbide precipitation along with partial recovery of martensite. The morphology of TM kept on changing while moving away from Ac1 towards the BM as the fraction of broken appearance was reduced and the sub-micron particles became finer. SEM observations resulted in good agreement with the nanohardness of the TM phase along the sub-critical HAZ. In contrast, microhardness results suggested the termination of tempering at a shorter distance with respect to Ac1 and hence a reduced extension of the softening region. The improved resolution for assessing softening through nanoindentation was due to the possibility of avoiding the contribution of the phase boundaries because of the smaller size of the indentation; this also permitted evaluation of TM at low peak temperatures far from Ac1 where early stages of tempering took place.
机译:电阻点焊双相钢的贱金属(BM)和热影响区(HAZ)已通过纳米压痕硬度测试进行了评估。在BM上探索了三种不同的表面条件,以评估纳米硬度响应。已通过在距较低临界温度Ac 1 线不同距离的各个相(例如铁素体和回火马氏体(TM))上进行纳米压痕研究了沿亚临界HAZ的软化。在TM上始终在距Ac 1 线100μm处发现破碎的外观和亚微米颗粒,表明碳化物沉淀以及马氏体的部分回收。当从Ac 1 移向BM时,TM的形态不断变化,这是因为减少了断裂外观的比例,并且亚微米颗粒变得更细。 SEM观察结果与沿亚临界热影响区的TM相的纳米硬度有很好的一致性。相反,显微硬度结果表明,相对于Ac 1 ,在较短的距离处回火终止,因此软化区域的延伸减少。通过纳米压痕评估软化的改进分辨率是由于避免了压痕尺寸的减小而避免了相界的影响。这还允许在远离回火早期的Ac 1 的低峰值温度下评估TM。

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