首页> 外文期刊>Journal of inorganic and organometallic polymers and materials >Effect of Zinc Content on Structural, Functional, Morphological, Resonance, Thermal and Magnetic Properties of Co_(1-x)Zn_xFe_2O_4/PVP Nanocomposites
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Effect of Zinc Content on Structural, Functional, Morphological, Resonance, Thermal and Magnetic Properties of Co_(1-x)Zn_xFe_2O_4/PVP Nanocomposites

机译:锌含量对Co_(1-x)Zn_xFe_2O_4 / PVP纳米复合材料的结构,功能,形态,共振,热和磁性能的影响

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摘要

Integrate Zinc substituted cobalt ferrites have incorporated by the Co-precipitation technique. The XRD pattern shows the formation and microstructure evolutions of nanocomposites. Cationic coordination, exchange interactions raised between the tetrahedral site in high frequency and octahedral site in the lower frequency described FTIR results. The SEM images showed that the spongy morphology with PVP matrix and fewer agglomerated grains. It exposes the grains and the range of grains recovered from 1 mu to 400 nm, which is in compromise with the test of grain size of XRD. VSM study reveals that the magnetization of substances raises by incrementing the non-magnetic (Zn) material incorporated cobalt ferrite. EPR confirmed that synthesized materials exhibited ferromagnetic properties from Lande g-factor. TGA/DSC curve reports the weight loss and heat flow by endothermic absorption through exothermic emission in the ferrite. It used these materials for the potential effort like magneto-optical recording media and magnetic sensors.
机译:通过共沉淀技术结合了整合锌取代的钴铁氧体。 XRD图谱显示了纳米复合材料的形成和微观结构的演变。 FTIR结果表明,阳离子配位,高频的四面体位点和低频的八面体位点之间产生交换相互作用。扫描电镜(SEM)图像显示PVP基体为海绵状,团聚颗粒较少。它暴露出晶粒和从1微米到400纳米恢复的晶粒范围,这与XRD晶粒尺寸的测试相矛盾。 VSM研究表明,物质的磁化强度通过增加掺入钴铁氧体的非磁性(Zn)材料而提高。 EPR证实合成材料具有Lande g因子的铁磁特性。 TGA / DSC曲线报告了铁氧体中放热吸收引起的吸热吸收引起的重量损失和热流。它使用这些材料来进行潜在的工作,例如磁光记录介质和磁传感器。

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