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Characterization of BaSnO_3 Powder Obtained by a Modified Sol-Gel Route

机译:改性溶胶-凝胶法获得的BaSnO_3粉末的表征

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摘要

A modified sol-gel method is used to prepare stoi- chiometric, homogeneous barium stannate powders. The synthesis process is described in detail in this Paper. One of the main characteristics of this Process is that monophasic powders are obtained Easily at low temperature (1000 deg. C). The resulting Powders are characterized by several methods such As X-ray diffraction, scanning electron microscopy, X-ray analysis, infrared spectroscopy and thermo- Gravimetric analysis. The different characterizations Allow us to conclude that powders obtained by this Method contain no impurity. These conclusions Show that this process is ideal for obtaining fine Powders that will give dense ceramics.
机译:改良的溶胶-凝胶法用于制备化学计量的均匀锡酸钡粉末。本文详细介绍了合成过程。该方法的主要特征之一是在低温(1000℃)下容易获得单相粉末。所得粉末通过几种方法进行表征,例如X射线衍射,扫描电子显微镜,X射线分析,红外光谱和热重分析。不同的特征使我们可以得出结论,用此方法获得的粉末不含杂质。这些结论表明,该方法对于获得能够产生致密陶瓷的细粉是理想的。

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