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Rapid method for determination of ~(90)Sr in biological samples by liquid scintillation counting after separation on synthesized column

机译:合成柱分离后液体闪烁计数快速测定生物样品中〜(90)Sr

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摘要

A simple, rapid and cost-efficient method for determination of activity concentration of Sr-90 in biological samples with an extraction chromatographic column (crown ether on teflon powder) and following counted by liquid scintillation counting was developed in this paper. The column retained most of Sr-90 while almost all of matrix ions were removed during rinsing steps with 8M nitric acid and finally Sr-90 was eluted with deionized water, the chemical recovery of strontium is greater than 60%, almost all of matrix ions were removed by the procedure we reported. Finally the uncertainty was evaluated and minimum detectable activity of this method is 1.28Bq/kg.
机译:本文建立了一种简单,快速,经济高效的方法,采用萃取色谱柱(聚四氟乙烯粉末上的冠醚)测定生物样品中Sr-90的活性浓度,然后通过液体闪烁计数法进行计数。该柱保留了大部分Sr-90,而在用8M硝酸冲洗的过程中几乎除去了所有基质离子,最后用去离子水洗脱了Sr-90,锶的化学回收率大于60%,几乎所有基质离子已通过我们报告的程序删除。最后,对不确定度进行了评估,该方法的最低可检测活性为1.28Bq / kg。

著录项

  • 来源
    《Journal of Environmental Radioactivity》 |2018年第2018期|15-19|共5页
  • 作者单位

    Chinese Ctr Dis Control & Prevent, Natl Inst Radiol Protect, China CDC Key Lab Radiol Protect & Nucl Emergency, Beijing, Peoples R China;

    Minist Ecol & Environm Peoples Republ China, Nucl & Radiat Safety Ctr, Beijing, Peoples R China;

    Chinese Ctr Dis Control & Prevent, Natl Inst Radiol Protect, China CDC Key Lab Radiol Protect & Nucl Emergency, Beijing, Peoples R China;

    Chinese Ctr Dis Control & Prevent, Natl Inst Radiol Protect, China CDC Key Lab Radiol Protect & Nucl Emergency, Beijing, Peoples R China;

    Chinese Ctr Dis Control & Prevent, Natl Inst Radiol Protect, China CDC Key Lab Radiol Protect & Nucl Emergency, Beijing, Peoples R China;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);美国《化学文摘》(CA);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Strontium 90; Liquid scintillation counting; Extraction chromatography; Uncertainty;

    机译:锶90;液体闪烁计数;萃取色谱法;不确定度;

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