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Controlled Synthesis of BaTiO_3-Coated Multiwall Carbon Nanotubes

机译:BaTiO_3包覆的多壁碳纳米管的受控合成

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摘要

We report the success in synthesis of BaTiO_3 (BTO) coating on acid-treated functionalized multiwall carbon nanotubes (MWCNTs). Functionalization treatment, coating temperature, and coating time were optimized in order to obtain the dense coating of BTO. Contact angle measurements were conducted on MWCNT surface to quantify the effectiveness of functionalization and were correlated with percentage coating. Coating thickness in the range of 5-15 nm was confirmed by using high-resolution transmission electron microscopy. X-ray photoelec-tron spectroscopy was used to confirm the formation of BTO perovskite phase. Microstructural characterization and elemental analysis were performed using scanning electron microscopy and energy-dispersive spectroscopy to confirm the homogeneous coating with high yield. Possible application of these fully coated MWCNTs can be in flexible pressure sensors.
机译:我们报告了在酸处理的功能化多壁碳纳米管(MWCNTs)上合成BaTiO_3(BTO)涂层的成功。优化功能化处理,涂覆温度和涂覆时间,以获得致密的BTO涂层。在MWCNT表面上进行接触角测量以量化功能化的有效性,并与涂覆百分比相关。通过使用高分辨率透射电子显微镜确认涂层厚度在5-15nm范围内。用X射线光电子能谱确认BTO钙钛矿相的形成。使用扫描电子显微镜和能量分散光谱进行了微结构表征和元素分析,以确认高产率的均匀涂层。这些完全覆盖的MWCNT的可能应用可能是在柔性压力传感器中。

著录项

  • 来源
    《Journal of the American Ceramic Society》 |2010年第11期|p.3618-3623|共6页
  • 作者单位

    Center for Energy Harvesting Materials and Systems (CEHMS), Institute for Critical Technology and Applied Science(ICTAS), Virginia Tech, Blacksburg, Virginia 24061;

    rnCenter for Energy Harvesting Materials and Systems (CEHMS), Institute for Critical Technology and Applied Science(ICTAS), Virginia Tech, Blacksburg, Virginia 24061;

    rnCenter for Energy Harvesting Materials and Systems (CEHMS), Institute for Critical Technology and Applied Science(ICTAS), Virginia Tech, Blacksburg, Virginia 24061;

    rnCenter for Energy Harvesting Materials and Systems (CEHMS), Institute for Critical Technology and Applied Science(ICTAS), Virginia Tech, Blacksburg, Virginia 24061;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);美国《生物学医学文摘》(MEDLINE);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

  • 入库时间 2022-08-17 13:40:38

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