Natural abundance 33S NMR spectroscopy. The first spectra of several major compound types

摘要

Using a high field, high power instrument, n33nS NMR spectra have been obtained for several previously unobservablencompound types including an aromatic isothiocyanate, a thiocyanate, a thiophenol, an alkyl aryl sulfide, a thiazole,na persulfate, a sulfinic acid and sulfinate salts, a sulfonhydrazide and a sulfinyl halide. The range of data for sulfonylnfluorides and chlorides has also been extended considerably.