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Transient heat transfer characteristic of silica aerogel insulating material considering its endothermic reaction

机译:考虑吸热反应的二氧化硅气凝胶绝缘材料的瞬态传热特性

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摘要

In the current work, we present an experimental study to investigate the reaction mechanism of silica aerogel material at high temperature. The experimental study is based on simultaneous thermal analyzer 449F3 as well as Fourier Transform Infrared Spectroscopy(FTIR). The results show that when the material is exposed at high temperature, the mass of material will decrease about 1.98% accompanying with endothermic effect. Via FTIR analysis, it is found that the mass loss of material may be caused by the removal of adsorbed water. Besides the experimental study, a numerical heat transfer model is constructed to study the transient heat transfer characteristic of aerogel material by taking the endothermic reaction into account. The numerical heat transfer model is validated by a classical Stefan problem and a corresponding experimental measurement. Afterwards, a parametric study is conducted to investigate the effect of two parameters, reaction temperature and reaction heat, on transient heat transfer characteristics of aerogel insulating material. The results show that:(1)Before reaching the reaction temperature T_(reaction), the material that with lower T_(reaction)possesses lower temperature. However, when it exceeds the reaction temperature, the material shows the highest temperature among other materials.(2)With the increase of reaction heat, the increasing trend of temperature is weakened and the emergent of the turning point that separates the temperature platform and temperature-rise period appears later.
机译:在目前的工作中,我们提出了一项实验研究,以研究二氧化硅气凝胶材料在高温下的反应机理。实验研究基于同步热分析仪449F3以及傅立叶变换红外光谱(FTIR)。结果表明,当材料在高温下暴露时,材料的质量将减少约1.98%,并伴有吸热作用。通过FTIR分析,发现材料的质量损失可能是由于去除了吸附的水而引起的。除实验研究外,还建立了数值传热模型,通过考虑吸热反应来研究气凝胶材料的瞬态传热特性。数值传热模型通过经典的Stefan问题和相应的实验测量得到验证。之后,进行了参数研究,研究了反应温度和反应热这两个参数对气凝胶绝热材料瞬态传热特性的影响。结果表明:(1)在达到反应温度T_(反应)之前,具有较低T_(反应)的材料具有较低的温度。然而,当温度超过反应温度时,该材料便是其他材料中温度最高的。(2)随着反应热的增加,温度的升高趋势减弱,并且出现了分离温度平台和温度的转折点。 -上升期稍后出现。

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  • 作者单位

    Key Laboratory of Thermo-Fluid Science and Engineering of MOE, School of Energy and Power Engineering, Xi'an Jiaotong University, Xi'an, Shaanxi 710049, PR China;

    Key Laboratory of Thermo-Fluid Science and Engineering of MOE, School of Energy and Power Engineering, Xi'an Jiaotong University, Xi'an, Shaanxi 710049, PR China;

    Key Laboratory of Thermo-Fluid Science and Engineering of MOE, School of Energy and Power Engineering, Xi'an Jiaotong University, Xi'an, Shaanxi 710049, PR China;

    Beijing Institute of Nearspace Vehicle's Systems Engineering, Beijing 100076, PR China;

    Beijing Institute of Nearspace Vehicle's Systems Engineering, Beijing 100076, PR China;

  • 收录信息 美国《科学引文索引》(SCI);美国《工程索引》(EI);
  • 原文格式 PDF
  • 正文语种 eng
  • 中图分类
  • 关键词

    Aerogel insulating material; Endothermic reaction; Transient heat transfer characteristics; Numerical model;

    机译:气凝胶绝缘材料;吸热反应;瞬态传热特性;数值模型;

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