Crack formation and microstructure-sensitive propagation in low cycle fatigue of a polycrystalline nickel-based superalloy with different heat treatments

摘要

Graphical abstractDisplay OmittedHighlights•Fractography of LCF experiments at room temperature was analyzed in detail.•Stress concentration around casting micropore was analyzed by X-ray CT and FEM.•Combination of micropore and precipitates dominates the LCF crack initiation behaviors.•Effects of heat treatment process on the LCF of a superalloy was summarized.AbstractGas turbine engine materials demand high performance of fatigue life under alternative loading. In this paper, crack initiation and propagation in the low cycle fatigue (LCF) of a polycrystalline nickel based superalloys was studied via experimental and numerical methods. LCF experiments were conducted with the specimens subjected to different heat treatment regimes, including of standard heat treatment (SHT), heat isostatic pressing (HIP), and combined heat treatment (HIP+SHT). Simulations based on finite element method (FEM) were implemented with the 3D digital model obtained from synchrotron radiation X-ray computerized tomography (CT) to investigate the effect of microporosity. Results indicated that microporosity was a dominant factor of fatigue crack and the parameters of microporosity including of porosity, effective diameter, and distribution co-contributed to affect fatigue life. The δ stack and carbide were observed to be fatigue crack sites. The HIP specimen had long fatigue cycle life since casting pore and acicular δ were eliminated, while further SHT can reintroduce δ into matrix resulting in high strength and low fatigue life. LCF crack behaviors in HIP+SHT superalloy depended on surface quality, stress concentration, and the quantity of carbide.