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High-Temperature Cermet Material Based on Intermetallic Nickel Matrix

机译:基于金属间镍基质的高温金属陶瓷材料

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摘要

A method for synthesis of an intermetallic nickel matrix reinforced with particles of different refractory compounds added at different concentrations is considered. Prepared materials are based on two variants of a Ni_3Al-Cr-W-Mo-Ti-Hf alloy: type VKNA- 1V alloy and type VKNA- 1V alloy with increased tungsten content (VKNA-lV(W)). The intermetallic matrix is reinforced with nanoparticles of the oxides Al_2O_3, Al_2O_3 • Y_2O_3, and Al_2O_3 • Y_2O_3 • HfO_2, with the content of reinforcing component at 2 and 5 vol %. Samples are compacted by spark plasma sintering. The microstructure of prepared cermet materials (CMs) is investigated using scanning electron microscopy. The impact viscosity and flexural strength are determined. We establish the effect that the content and composition of the reinforcing component has on the physicomechanical properties of the high-temperature CMs based on an intermetallic matrix dispersion-hardened with refractory metal particles. Our findings show that the optimal combination of flexural strength and impact viscosity at room temperature is achieved in the CM sample in which the intermetallic matrix is based on VKNA-1V(W) alloy and the reinforcing component is represented by ternary oxide Al_2O_3 • Y_2O_3 • HfO_2 added at a concentration of 2%.
机译:考虑了用不同浓度添加的不同耐火化合物颗粒合成增强的金属间镍基质的方法。制备的材料基于Ni_3Al-Cr-W-Mo-Ti-Hf合金的两个变体:型VKNA-1V合金和型VKNA-1V合金,具有增加的钨含量(VKNA-LV(W))。将金属间基质用氧化物Al_2O_3,Al_2O_3•Y_2O_3和Al_2O_3•Y_2O_3•HFO_2的纳米颗粒增强,其含量为2和5体积%。样品被火花等离子体烧结压实。使用扫描电子显微镜研究制备的金属陶瓷材料(CMS)的微观结构。确定冲击粘度和弯曲强度。我们建立了增强组分的含量和组成对高温CMS的物理机械性能,基于耐火金属颗粒硬化的金属间基质分散体。我们的研究结果表明,在室温下的弯曲强度和冲击粘度的最佳组合在其中金属间基质基于VKNA-1V(W)合金,加强组分由三元氧化物Al_2O_3•Y_2O_3表示HFO_2以2%的浓度添加。

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