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An empirical method to estimate the viscosity of mineral oil by means of ultrasonic attenuation

机译:一种通过超声衰减估算矿物油粘度的经验方法

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摘要

This paper presents an empirical method for measuring the viscosity of mineral oil. In a built-in pipeline application, conventional ultrasonic methods using shear reflectance or rheological and acoustical phenomena may fail because of attenuated shear wave propagation and an unpredictable spreading loss caused by protective housings and comparable main flows. The empirical method utilizing longitudinal waves eliminates the unknown spreading loss from attenuation measurements on the object fluid by removing the normalized spreading loss per focal length with the measurement of a reference fluid of a known acoustic absorption coefficient. The ultrasonic attenuation of fresh water as the reference fluid and mineral oil as the object fluid were measured along with the sound speed and effective frequency. The empirical equation for the spreading loss in the reference fluid is determined by high-order polynomial fitting. To estimate the shear viscosity of the mineral oil, a linear fit is applied to the total loss difference between the two fluids, whose slope (the absorption coefficient) is combined with an assumed shear-to-volume viscosity relation. The empirical method predicted the viscosities of two types of the mineral oil with a maximum statistical uncertainty of 8.8% and a maximum systematic error of 12.5% compared with directly measured viscosity using a glass-type viscometer. The validity of this method was examined by comparison with the results from theoretical far-field spreading.
机译:本文提出了一种测量矿物油粘度的经验方法。在内置管道应用中,使用剪切反射率或流变和声学现象的常规超声方法可能会因剪切波传播衰减以及保护性外壳和相当的主流导致不可预测的扩展损失而失败。利用纵波的经验方法通过用已知吸声系数的参考流体的测量值去除每焦距的归一化扩展损耗,从而消除了对目标流体的衰减测量中的未知扩展损耗。测量了作为参考流体的淡水和作为目标流体的矿物油的超声衰减,以及声速和有效频率。通过高阶多项式拟合确定参考流体中扩散损失的经验方程式。为了估算矿物油的剪切粘度,将线性拟合应用于两种流体之间的总损耗差,将其斜率(吸收系数)与假定的剪切体积粘度关系结合起来。经验方法与使用玻璃型粘度计直接测量的粘度相比,预测了两种矿物油的粘度,其最大统计不确定性为8.8%,最大系统误差为12.5%。通过与理论远场扩展的结果进行比较,检验了该方法的有效性。

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