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Leak tight joint procedures for ODS-Cu/ODS-Cu by the advanced brazing technique

机译:通过先进的钎焊技术对ODS-Cu / ODS-Cu进行密封连接

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The joint of the oxide dispersion strengthened copper alloy, ODS-Cu (ODS-Cu/ODS-Cu), was prepared. The applied ODS-Cu was GlidCop (R) (Cu-0.3 wt%Al2O3). The joint procedures were based on the brazing technique between GlidCop (R) and tungsten (W) with BNi-6 (Ni-11%P) filler material. This method was performed without compressive load and without any intermediate layer, and was named the advanced brazing technique. In this study, first, the joint GlidCop (R)/GlidCop (R) was prepared without any compressive load. The joint was subjected to the three-point bending test, the Vickers hardness test, microstructure observation and the leak tightness test. The yield strength of the joint was approximately one-half of that of the GlidCop (R) bulk. In addition, the joint was not leak tightness against fluids. Next, the joint was prepared with compressive load of (similar to)0.54 MPa which was applied in the direction perpendicular to the joint interface. The yield strength of the joint was almost as high as that of the GlidCop (R) bulk. Furthermore, the joint achieved leak tightness against fluids. The special feature of this joint method is that a limited volume of the GlidCop (R) surfaces near the bonding interface are melted during the bonding heat treatment phase at 960 degrees C due to the eutectic reaction of the Cu-P system. Then, after finalizing the solidification, a tight bonding layer are created without any cavities and cracks. This phenomenon seems to resemble a micro scale welding. The present brazing technique can promise fabrication of a high heat flux component with a complex shaped fluid flow path system with leak tightness.
机译:制备了氧化物弥散强化铜合金ODS-Cu(ODS-Cu / ODS-Cu)的接头。所施加的ODS-Cu为GlidCop(R)(Cu-0.3重量%Al 2 O 3)。联合程序基于使用BNi-6(Ni-11%P)填充材料的GlidCop(R)和钨(W)之间的钎焊技术。该方法在没有压缩载荷且没有任何中间层的情况下执行,被称为高级钎焊技术。在这项研究中,首先,准备没有任何压缩载荷的关节GlidCop(R)/ GlidCop(R)。对接头进行三点弯曲测试,维氏硬度测试,显微组织观察和密封性测试。接头的屈服强度约为GlidCop(R)本体的屈服强度的一半。另外,该接头没有对流体的密封性。接下来,以垂直于接头界面的方向施加(近似)0.54MPa的压缩载荷制备接头。接头的屈服强度几乎与GlidCop本体的屈服强度一样高。此外,接头实现了对流体的密封性。这种联合方法的特殊之处在于,由于Cu-P体系的共晶反应,在960摄氏度的键合热处理阶段,有限体积的键合界面附近的GlidCop(R)表面熔化。然后,在完成固化后,形成紧密的粘结层,而没有任何空腔和裂纹。这种现象似乎类似于微型焊接。本发明的钎焊技术可以保证具有复杂形状的具有密封性的流体流动路径系统的高热通量部件的制造。

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