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Effect of Fiber Chemical Treatments on Performance of Date Palm Fibers Using Response Surface Methodology

机译:响应面法研究纤维化学处理对枣棕纤维性能的影响

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The objective of this study is to investigate the effect of optimized alkali treatment on the lignin reduction of date palm fibers. This kind of fiber treatment is used to improve the performance of natural fibers. The experiments conducted by central composite design (CCD) through response surface methodology (RSM) with four independent factors, each at five levels. Raw fibers underwent a surface modification method by alkali treatment with four independent variables, hydrogen peroxide (2-6 wt %), sodium hydroxide (3-7 wt %), temperature (30-46 degrees C), and treatment time (14-18 h). The Fourier transform infrared spectroscopy, tensile properties, and thermal gravimetry analysis of untreated, treated, and optimized treated fibers were investigated. The results showed that the optimized levels for hydrogen peroxide and sodium hydroxide were 4.9 and 5.2 wt %. The optimum temperature and treatment time were found to be 38.8 degrees C and 17.8 h, respectively. At the optimized values of the independent variables, the lignin content of the fibers was 10.11%. Meantime, the tensile test results show that alkali treatment with optimized values improves the performance of fibers, although no high values are obtained. (c) 2019 American Institute of Chemical Engineers Environ Prog, 38:e13146, 2019
机译:这项研究的目的是研究优化的碱处理对椰枣纤维木质素还原的影响。这种纤维处理用于改善天然纤维的性能。由中央复合设计(CCD)通过响应表面方法(RSM)进行的实验,具有四个独立的因素,每个因素在五个层次上。粗纤维通过碱处理进行表面改性,方法包括四个独立变量:过氧化氢(2-6 wt%),氢氧化钠(3-7 wt%),温度(30-46摄氏度)和处理时间(14- 18小时)。研究了未处理,处理和优化处理过的纤维的傅里叶变换红外光谱,拉伸性能和热重分析。结果表明,过氧化氢和氢氧化钠的最佳含量为4.9和5.2重量%。发现最佳温度和处理时间分别为38.8℃和17.8h。在自变量的最佳值下,纤维的木质素含量为10.11%。同时,拉伸试验结果表明,尽管没有获得高值,但以最佳值进行碱处理可以改善纤维的性能。 (c)2019美国化学工程师学会Environ Prog,38:e13146,2019

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