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Effect of Ni-doping on the structural and optical properties of ZnO nanoparticles prepared by chemical precipitation method

机译:Ni-掺杂对化学沉淀法制备ZnO纳米粒子结构和光学性质的影响

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Undoped ZnO nano particles and Ni doped ZnO nanoparticles prepared by chemical precipitation method and assessed for their structural, morphological and optical properties. The prepared undoped and Ni doped ZnO nanoparticles were characterized by using X-ray diffraction (XRD), Fourier transform infrared spectral (FTIR), UV-Visible spectrophotometer, Scanning electron microscopy (SEM) and Energy Dispersive X-ray analysis (EDAX), Photoluminescence spectra (PL). XRD pattern shows the purity of prepared undoped and Ni doped ZnO nanoparticles size. Scanning electron microscopy (SEM) observations revealed remarkable change in morphology of the prepared samples. The presence of functional groups and chemical bonding was confirmed by FTIR and UV analysis. The defect states were revealed from the UV and visible emissions of the photoluminescence spectra.
机译:未掺杂的ZnO纳米颗粒和Ni掺杂的ZnO纳米颗粒通过化学沉淀法制制备,并评估其结构,形态和光学性质。通过使用X射线衍射(XRD),傅里叶变换红外光谱(FTIR),UV可见分光光度计,扫描电子显微镜(SEM)和能量分散X射线分析(EDAX),表征制备的未掺杂和Ni掺杂的ZnO纳米颗粒。光致发光光谱(PL)。 XRD图案显示所制备的未掺杂和Ni掺杂ZnO纳米粒子尺寸的纯度。扫描电子显微镜(SEM)观察结果显示了制备样品的形态的显着变化。通过FTIR和UV分析证实了官能团和化学键合的存在。从光致发光光谱的UV和可见排放中揭示了缺陷状态。

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