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Formation of equiaxed grains in selective laser melted pure titanium during annealing

机译:在退火期间在选择性激光熔化纯钛中形成等轴晶粒的形成

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Commercially pure titanium (CP-Ti) has seen major applications in biomedical equipment. The use of selective laser melting (SLM) has become more common concerning the fabrication of CP-Ti components with a complicated shape in biomedical implants, where high strength and ductility are required. However, SLM manufactured CP-Ti often exhibits high strength and low ductility, as well as mechanical anisotropy because SLM process typically results in the formation of long columnar grains comprising of fine acicular α′ martensite. Heat treatment must be preceded to transform the acicular α′ to equiaxed α grain. This study demonstrated that annealing at 650?°C of SLM CP-Ti can create an equiaxed structure, resulting in a weakened texture. The formation of equiaxed grains occurred at two types of microstructural features, acicular α′ and irregular massive (α′m) martensite, which exhibited different sizes, morphologies, and contained different types of substructures under SLM as-fabricated condition. The formation mechanism of equiaxed grains in the α′ region is dominated by the coalescence of acicular α′ of the same variant and the dissolution of α′ into the matrix, whereas the formation mechanism in the α′mregion is primarily dominated by the growth of the preexisting subgrains. A small number of equiaxed grains with new orientations were formed in the α′mregion. The majority of equiaxed grains were formed in the acicular α′ region and inherited the grain orientations of the preexisting α′ or matrix. Therefore, a similar but weakened texture was inherited from the microstructure of the SLM CP-Ti after annealing.
机译:商业纯钛(CP-TI)在生物医学设备中看到了主要应用。选择性激光熔化(SLM)的使用更常见于在生物医学植入物中具有复杂形状的CP-Ti组分的制造更常见,其中需要高强度和延展性。然而,SLM制造的CP-TI通常具有高强度和低延展性,以及机械各向异性,因为SLM工艺通常导致长柱状颗粒,其包含精细针状α'马氏体。必须先使用热处理以将针状α'转变为等轴α颗粒。本研究证明,在650°C的SLM CP-Ti的退火可以产生等式结构,导致质地削弱。等式晶粒的形成发生在两种类型的微观结构特征,针状α'和不规则的大规模(α'm)马氏体上,其表现出不同的尺寸,形态,并在SLM以制造条件下包含不同类型的子结构。 α'区域的等轴晶粒的形成机制由α'相同变体的纤维α'的聚焦和α'溶解到基质中,而α的形成机制主要由生长主导预先存在的亚征。在α的物质中形成少量具有新取向的等轴晶粒。大多数等轴晶粒在针状α'区域中形成并遗传了预先存在的α'或基质的晶粒取向。因此,从退火后的SLM CP-TI的微观结构继承了类似但弱化的纹理。

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