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The effect of sintering on the properties of magnesia-granite sludge ceramics shaped by temperature-induced forming

机译:烧结对温度诱导成形镁质污泥陶瓷晶体性能的影响

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Recycling waste materials have attracted considerable attention owing to the increased interest in depressing the negative impact on the environment. The present work investigates the effect of increasing the granite sludge-waste materials from granite manufacture-on the physical, mechanical and electrical properties of magnesia ceramics. The temperature-induced forming (TIF) method is used to shape magnesia-granite sludge ceramics. The sintered ceramics are characterized by XRD and SEM, in addition to measuring the bulk density, apparent porosity, linear shrinkage, microhardness, and electrical resistivity. Sintering of magnesia-granite bodies resulted in the formation of periclase-forsterite ceramics. The XRD results show that the forsterite phase increases reaching 78% at 40?wt% granite. The increase in granite sludge from 10 to 40?wt% increases the bulk density from 1.86 to 2.69?g/cm3and the apparent porosity decreases from 40 to 15%, respectively. Microhardness is improved by increasing the granite sludge wt% reaching 7.9?GPa. The microstructure of the formed periclase-forsterite is versatile with a rhombohedral structure for periclase and a flower structure for forsterite. The forsterite phase is formed by the diffusion of granite sludge into the formed periclase.
机译:由于对对环境的负面影响增加的兴趣增加,回收废料引起了相当大的关注。目前的工作调查了增加花岗岩污泥废料从花岗岩制造的效果 - 氧化镁陶瓷的物理,机械和电性能。温度诱导的成形(TIF)方法用于塑造氧化镁 - 花岗岩污泥陶瓷。烧结陶瓷的特征在于XRD和SEM,除了测量堆积密度,表观孔隙率,线性收缩,显微硬度和电阻率之外。氧化镁 - 花岗岩体的烧结导致形成蠕变型陶瓷陶瓷。 XRD结果表明,史氏峰相增加了40℃的达到78%的花岗岩。花岗岩污泥的增加从10至40℃的污泥增加增加了1.86至2.69Ω·克/厘米的堆积密度分别从40〜15%降低。通过增加花岗岩污泥wt%达到7.9μm≤GPA来改善微硬度。形成的Periclase-Forsterite的微观结构与蠕动叶片的裂纹结构和Forsterite的花结构是通用的。通过将花岗岩污泥的扩散到形成的蠕变形成的前馏石相。

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