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Rheological properties of irregular-shaped titanium-hydroxyapatite bimodal powder composite moulded by powder injection moulding

机译:粉末注射成型模制不规则形钛 - 羟基磷灰石双峰粉复合材料的流变性能

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This paper presents an alternative approach in powder injection moulding (PIM) process by highlighting the advantages of using irregular-shaped and bimodal size powder in Ti6Al4V-HA composite. An investigation on the rheological behaviour Ti6Al4V-HA feedstock at a ratio of 90:10 weight percent was done using spherical and irregular shapes of Ti6Al4V powder particle, together with palm stearin and polyethylene acts as a binder system. Subsequent to the rheological results, the critical powder volume percentage (CPVP) value of the bimodal feedstock improved by 5–8 vol. %. Furthermore, an irregular-shaped Ti6Al4V-HA shows pseudoplastic behaviour and low viscosity with the values of 73–408 Pa.s which is comparable with the spherical-shaped Ti6Al4V-HA (48–305 Pa.s). The injected parts of bimodal irregular-shaped Ti6Al4V-HA also successfully produced without any cracks and distortion with high relative density of 95% after sintering. The result is supported by SEM morphological images which displays micron size porosities that will benefit the sintered part as scaffold for a good osseointegration property with cells. The findings highlight the suitability of irregular-shaped Ti6Al4V-HA during injection moulding as it had outstanding rheological behaviour as good as spherical-shaped Ti6Al4V-HA. Sintered irregular-shaped Ti6Al4V-HA with porous morphological structure, suggest a useful alternative material of irregular morphology of Ti alloy in biomedical industries especially for bone implant application.
机译:本文通过在Ti6Al4V-HA复合材料中突出显示使用不规则形状和双峰尺寸粉末的优点,介绍了粉末注射成型(PIM)工艺的替代方法。使用Ti6Al4V粉末颗粒的球形和不规则形状与棕榈茎和聚乙烯作为粘合剂体系,使用球形和不规则的形状进行90:10重量%的流变学行为Ti6Al4V-HA原料的研究。在流变结果之后,双峰原料的临界粉末体积百分比(CPVP)值改善了5-8体积。 %。此外,不规则形状的Ti6Al4V-HA显示假塑性行为和低粘度,其值为73-408Pa。与球形Ti6Al4V-Ha(48-305Pa)相当。双峰不规则形状的Ti6A14V-HA的注入部分也在烧结后没有任何裂缝和畸变的裂缝和变形,高相对密度为95%。结果由SEM形态图像支持,其显示微米尺寸的孔隙率,其将烧结部件有益于与细胞的良好骨整合性的支架。该发现突出了注塑成型期间不规则形状的Ti6Al4V-HA的适用性,因为它具有出色的流变行为与球形Ti6Al4V-HA一样好。烧结不规则形状的Ti6Al4V-HA具有多孔形态结构,表明了生物医学行业中Ti合金的不规则形态的有用替代材料,特别是对于骨植入物应用。

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