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Comparison of RF and Pulsed Magnetron Sputtering for the Deposition of AZO Thin Films on PET

机译:RF和脉冲磁控溅射在宠物沉积铝薄膜沉积中的比较

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AZO thin films (around 200 nm thick) were grown on polyethylene terephthalate (PET) at room temperature. The plasma was activated using a 13.56 MHz (RF) or a 15 kHz pulsed (PMS) source at a power of 60 W. Optical reflection and transmittance were measured using a UV-Vis-NIR spectrometer over the wavelengths from 190 nm to 2500 nm. All samples show average transmittances greater than 83% in the visible region. The electrical resistivity was measured by the linear four-point probe method to be around 0.001 Ωcm for 200 nm-thick AZO films grown by PMS. XRD results indicated that the films had a hexagonal wurtzite structure and were preferentially oriented in the (002) plane. The surface morphology of the AZO thin films was characterized using Scanning Electron Microscopy (SEM); film chemical composition was studied using Energy Dispersive X-ray Spectroscopy (EDS). For this, an EDS coupled to the Scanning Electron Microscope was used. Only for films grown by PMS were no cracks observed.
机译:在室温下在聚对苯二甲酸乙二醇酯(PET)上生长偶氮薄膜(约200nm厚)。使用13.56MHz(RF)或15kHz脉冲(PMS)源以60W的功率激活等离子体。使用从190nm至2500nm的波长上使用UV-Vis-Nir光谱仪测量光学反射和透射率。所有样品显示在可见区域中的平均透射率大于83%。通过线性的四点探针方法测量电阻率为200nm厚的偶氮膜的约0.001Ωcm。 XRD结果表明,薄膜具有六边形紫斑岩结构,优先于(002)平面中取向。使用扫描电子显微镜(SEM)表征偶氮薄膜的表面形态;使用能量分散X射线光谱(EDS)研究薄膜化学成分。为此,使用耦合到扫描电子显微镜的EDS。仅针对PMS生长的薄膜未观察到裂缝。

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