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Study on the Structure and Properties of Continuous Basalt Fibres

机译:连续玄武岩纤维的结构与性能研究

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The chemical composition, X-ray diffraction, thermal properties, flammability, mechanical properties and morphology of basalt fibres are investigated in this paper. Chemical analysis and energy dispersive X-ray fluorescence spectrometer experiments showed that basalt fibre is a kind of aluminosillicate fibre which is mainly composed of oxides such as SiO2, Al2O3, Fe2O3, CaO, MgO, Na2O, K2O, P2O5 and so on. X-ray diffraction indicated that the bulk structure of the fibres is non-crystal with a short range order but no long range order. SEM observation found that basalt fibre is circular in cross-section and smooth in the longitudinal direction. Solubility experiments revealed the superior resistance of the fibre to acids, alkaline and organic solvents. DGA demonstrated there are three weight loss stages in the process of elevating temperature. They are, respectively, evaporation of moisture in the fibre at about 100?°C, decomposition of the residual carbonate minerals between 480?°C and 630?°C, and decomposition of newly generated carbonates between 850~995?°C. On the heat flow curve, there are also three endothermic peaks, where the first and second correspond to the last two stages of weight loss and the third to the melting process of the fibre, whose onset is from 1122.14?°C, reaching a peak value at 1194.96?°C, and ending at 1380?°C. The tensile strength of basalt filaments and staple fibre was measured. Tensile and shear properties of the fibre were also tested.
机译:本文研究了化学成分,X射线衍射,热性质,易燃性,机械性能和形态。化学分析和能量色散X射线荧光光谱仪实验表明,玄武岩纤维是一种铝硅酸盐纤维,主要由SiO 2,Al2O3,Fe 2 O 3,CaO,MgO,Na 2 O,K 2 O,P2O5等组成。 X射线衍射表明,纤维的堆积结构是非晶体,短距离,但没有长的级顺序。 SEM观察发现,玄武岩纤维在横截面中是圆形的,沿纵向光滑。溶解度实验揭示了纤维对酸,碱性和有机溶剂的优异抗性。 DGA证明了在温度升高过程中存在三个重量损失阶段。它们分别在纤维中蒸发纤维在约100?℃下,在480℃和630℃之间的残留碳酸盐矿物的分解,并在850〜995Ω℃之间分解新产生的碳酸盐。在热流曲线上,还存在三个吸热峰,其中第一和第二对应于减肥的最后两个阶段和第三个纤维的熔化过程,其起初是1122.14Ω·°C,到达峰值价值在1194.96?°C,并在1380℃结束。测量玄武岩长丝和短纤维的拉伸强度。还测试了纤维的拉伸和剪切性能。

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