首页> 外文期刊>International Journal of Renewable Energy Development >Biodiesel Production through Catalytic Microwave In-situ Transesterification of Micro-algae (Chlorella sp.)
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Biodiesel Production through Catalytic Microwave In-situ Transesterification of Micro-algae (Chlorella sp.)

机译:生物柴油通过催化微波原位酯交换来生产微藻(小球藻SP。)

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摘要

Aim of this research are to study and develop research related to the potential of Chlorella sp. into biodiesel with the help of microwaves in-situ transesterification by characterizing parameters such as microwave power (300; 450; 600 W) and reaction time (10; 30; 50 minutes) with catalyst concentration of KOH and molar ratio of microalga : methanol are 2% and 1:12 respectively and optimized by response surface methodology with Face Centered Central Composite Design (FCCCD). The study was carried out by dissolving the catalyst into methanol according to the variable which was then put into a reactor containing microalgae powder in the microwave and turned on according to the predetermined variable. After the reaction process is complete, the mixture is filtered and resuspended with methanol for 10 minutes to remove the remaining FAME and then the obtained filtrate is cooled. Water is added to the filtrate solution to facilitate the separation of hydrophilic components before being separated and pushed apart until 3 layers are formed. Amount of FAMEs in the first layer formed were extracted with n-hexane solution and washed with water and the FAME product obtained was then distilled to remove the remaining n hexane and then weighed. The results indicated that yield increased with increasing reaction time and microwave power with the best conditions of 50 minutes each and 440.53 watts with the highest yield reaching 35.72% (dry basis) through using of KOH catalysts with low concentrations, 2% .
机译:该研究的目的是研究和发展与小球藻潜力有关的研究。通过表征微波功率(300; 450; 600 W)和反应时间(10; 30; 50分钟)的参数,通过微波地原位酯交换,通过微波功率(300; 450; 600 W)和催化剂浓度的KOH和MOREGA的摩尔比的反应时间(10; 30; 50分钟)来看2%和1:12分别与响应面方法与面部居中中央复合设计(FCCCD)进行优化。通过将催化剂溶解在甲醇中,根据该变量将催化剂溶解在微波中的微藻粉末中的反应器中进行,并根据预定变量导通。反应过程完成后,将混合物过滤并用甲醇重悬10分钟以除去剩余的成本,然后冷却得到的滤液。将水加入到滤液溶液中以促进亲水组分在分离并被推动至形成3层之前分离。用正己烷溶液萃取形成的第一层中的含量的量,然后用水洗涤,然后蒸馏出来的MAME产物以除去剩余的N己烷,然后称重。结果表明,通过使用低浓度的KOH催化剂,每次和微波功率增加50分钟的最佳条件,最佳条件和微波功率增加了50分钟的最佳条件,其产量增加了50分钟的最佳条件,最高率为35.72%(干基)。

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