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Effect of Current Density on the Performance of Ni–P–ZrO2–CeO2 Composite Coatings Prepared by Jet-Electrodeposition

机译:电流密度对喷射电沉积制备的Ni-P-ZrO2-CeO2复合涂层性能的影响

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The objective of this study was to improve the surface properties, hardness, wear resistance and electrochemical corrosion resistance of #45 steel. To this end, Ni–P–ZrO2–CeO2 composite coatings were prepared on the surface of #45 steel using the jet-electrodeposition technique by varying the current density from 20 to 60 A/dm2. The effect of current density on the performance of the composite coatings was evaluated. Scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS) and X-ray diffraction (XRD) were applied to explore the surface topography, elemental composition, hardness and electrochemical corrosion resistance of the composite coatings. The results showed that with the increase in the current density, the hardness, wear resistance, and electrochemical corrosion resistance tends to increase first and then decrease. At a current density of 40 A/dm2, the hardness reached a maximum of 688.9 HV0.1, the corrosion current reached a minimum of 8.2501 × 10?5 A·cm?2, and the corrosion potential reached a maximum of ?0.45957 V. At these values, the performance of the composite coatings was optimal.
机译:本研究的目的是改善#45钢的表面性质,硬度,耐磨性和电化学耐腐蚀性。为此,通过将喷射电沉积技术从20至60a / dm2的电流密度改变,使用喷射电沉积技术在#45钢表面上制备Ni-P-ZrO2-CeO2复合涂层。评价电流密度对复合涂层性能的影响。扫描电子显微镜(SEM),能量分散X射线光谱(EDS)和X射线衍射(XRD)探讨复合涂层的表面形貌,元素组成,硬度和电化学耐腐蚀性。结果表明,随着电流密度的增加,硬度,耐磨性和电化学耐腐蚀性倾向于先增加,然后减少。在电流密度为40a / dm2,硬度最高达到688.9 hv0.1,腐蚀电流最小达到8.2501×10?5 a·cm?2,并且腐蚀电位最大达到?0.45957 V 。在这些值下,复合涂层的性能是最佳的。

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