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Preparation and characterization of diatomite and hydroxyapatite reinforced porous polyurethane foam biocomposites

机译:硅藻土和羟基磷灰石增强多孔多孔聚氨酯泡沫生物复合材料的制备及表征

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摘要

Porous three-dimensional (3D) polyurethane-based biocomposites were produced utilizing diatomite and hydroxyapatite as fillers. Diatomite and Hydroxyapatite (HA) were utilized to reinforce the morphological, chemical, mechanical, and thermal properties of polyurethane foam (PUF). Diatomite and Hydroxyapatite were added into polyurethane at variable percentages 0, 1, 2, and 5. The mechanical properties of PUF were analyzed by the compression test. According to the compression test results, the compressive strength of the polyurethane foam is highest in the reinforced foam at 1% by weight hydroxyapatite compared to other reinforced PUFs. Scanning electron microscopy (SEM) images presented structural differences on foam by adding fillers. Functional groups of PUF were defined by Fourier Transform Infrared Spectroscopy (FTIR) and the thermal behavior of PUF was studied with Thermogravimetric Analysis (TGA). The obtained results revealed that PUF/HA biocomposites indicated higher thermal degradation than PUF/Diatomite biocomposites.
机译:使用硅藻土和羟基磷灰石作为填料的多孔三维(3D)基于聚氨酯的生物复合材料。利用硅藻土和羟基磷灰石(HA)加强聚氨酯泡沫(PUF)的形态学,化学,机械和热性能。在可变百分比0,1,2和5的聚氨酯中加入硅藻土和羟基磷灰石。通过压缩试验分析PUF的机械性能。根据压缩试验结果,与其他增强的PUF相比,聚氨酯泡沫的压缩强度在增强泡沫中以1重量%重量的羟基磷灰石。扫描电子显微镜(SEM)图像通过添加填料呈现泡沫结构差异。 PUF的官能团由傅里叶变换红外光谱(FTIR)定义,并利用热重分析(TGA)研究了PUF的热行为。所得结果表明,PUF / HA生物复合材料表明比PUF /硅藻土生物复合材料更高的热降解。

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