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Preparation of graphene/Au aerogel film through the hydrothermal process and application for H2O2 detection

机译:通过水热过程制备石墨烯/ Au气凝胶膜及其对H2O2检测的应用

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摘要

In this paper, one-step preparation of graphene/gold nanoparticle hydrogel film through the hydrothermal method is reported. The hydrogel film could be formed on a glass substrate under hydrothermal conditions, and upon freeze-drying, the aerogel film of 40 μm thickness with satisfying flexibility and strength is obtained. The aerogel composite film is characterized by scanning/transmission electron microscopy, X-ray diffraction, Raman spectroscopy and X-ray photoelectron spectroscopy. Moreover, the aerogel film is directly used as the electrochemical electrode for sensing H _(2) O _(2) , and exhibits good performance with a broad linear range, low detection limit and excellent selectivity. This work provides a route for the fabrication of graphene film material with wide potential in various aspects.
机译:本文报道了通过水热法的石墨烯/金纳米粒子水凝胶膜的一步制备。水凝胶膜可以在水热条件下形成在玻璃基板上,并且在冷冻干燥时,获得40μm厚度柔韧性和强度的气凝胶膜。气凝胶复合薄膜的特征在于扫描/透射电子显微镜,X射线衍射,拉曼光谱和X射线光电子能谱。此外,气凝胶薄膜直接用作用于感测H _(2)O _(2)的电化学电极,并且具有宽线性范围,低检测极限和优异的选择性表现出良好的性能。这项工作提供了在各方面具有宽潜力的石墨烯薄膜材料的途径。

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