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Electroless Ni-P-ferrite composite coatings for microwave applications

机译:用于微波应用的化学镀Ni-p-铁氧体复合涂层

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摘要

Electroless, EL coating technique is one of the elegant ways of coating by controlling the temperature and pH of the coating bath in which there is no usage of electric current. It is estimated that the market for this chemistry will increase at a rate of about 15% per year. Use of microwave energy for synthesis of material with novel microstructures is an exciting new field in material science with enormous application.In this investigation, nanograined BaZn2-e?‘|Coe?‘|Fe16O27 (e?‘| = 0.0, 0.4, 0.8, 1.2, 1.6 and 2.0) powders have been synthesized by citrate precursor method followed by heat treatment at various specified temperatures like 650, 750 and 850?°C for 3 h in the furnace. In addition heat treatments are also carried out in the microwave oven of the power rating of 760 W. The powders thus produced have been characterized by SEM, EPMA, VSM, XRD and thermal analysis techniques.As a forward step towards EL nano-composite coatings, Ni-P-e?‘? (e?‘? = BaZn2-e?‘| Coe?‘|Fe16O27) coatings with thickness less than a?? 0.1 mm thick has been produced. Such coating exhibits absorption of microwave in the range of 12-18 GHz up to about 20 db depending upon the volume fraction of the ferrite particles embedded in the Ni-P matrix.
机译:通过控制没有电流的涂布浴的温度和pH,无电,EL涂布技术是涂覆的优雅涂层方式之一。据估计,这种化学市场将以每年约15%的速度增加。使用微波能量来合成具有新型微观结构的材料是具有巨大应用中的材料科学的令人兴奋的新领域。在巨大的应用中,纳米林Bazn2-e?''| COE?'| Fe16O27(E?'| = 0.0,0.4,0.8通过柠檬酸盐前体方法合成,1.2,1.6和2.0)粉末合成,然后在炉内以650,750和850Ω℃如650,750和850Ω℃进行热处理。此外,还在760W的额定功率的微波炉中进行热处理。如此生产的粉末的特征在于SEM,EPMA,VSM,XRD和热分析技术。朝向EL纳米复合涂层的前进步骤,Ni-Pe?'? (e?'?= bazn2-e?'| coe?'fe16o27)厚度小于a的涂层生产了0.1毫米厚。根据Ni-P基质中嵌入的铁氧体颗粒的体积分数,这种涂层在12-18GHz的范围内显示出微波的吸收。

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